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颗粒学报（英文版）
颗粒学报（英文版）

郭慕孙

双月刊

1674-2001

jcsp@home.ipe.ac.cn

010-82629146

100080

北京中关村北二条1号中科院过程所内

颗粒学报（英文版）/Journal China ParticuologyCSCDCSTPCD北大核心EISCI
查看更多>>本刊以创精品与国际化为办刊方针，旨在反映中国颗粒学研究的最新成果、及时追踪国际颗粒学领域的最新动态。学报主要刊登国内外颗粒学领域中的研究、工程和应用方面的优秀原始论文，包括颗粒测试与表征、颗粒制备与处理、流态化、气溶胶和超微颗粒等。本刊不仅设有论坛、研究论文、研究简报等内容，还有书评、会议信息与报道、测试仪器进展等栏目，便于相关人士进行学术交流，并为科技成果的展示提供平台，信息十分丰富。本刊已陆续被美国化学文摘（CA），俄罗斯文摘杂志（AJ），剑桥科学文摘（CSA）以及中国科技论文与引文数据库(CSTPCD)收录。China PARTICUOLOGY, a bimonthly interdisciplinary journal in English, purports to present the best papers in research, engineering and application in the overall field of PARTICUOLOGY, including particle characterization, particle preparation, aerosol, fluidization and ultra-fine particles. The word PARTICUOLOGY was coined to correspond to its Chinese terminology, which denotes both the science and technology of particles. Although the journal is China-based, it serves as a medium for all accepted papers of international origin, especially the best papers representing current advances in the world. Besides scientific and engineering papers, the journal includes the following sections: R & D notes, Current events, Editorials reviews, Forum for comments, opinions and qualified speculations, News on books, instruments and meetings.Now， China Particuology has been indexed by CA, AJ , CSA and CSTPCD.??读者对象（Audiences）： 中国颗粒学会会员、国内外从事颗粒学和颗粒技术研究和生产的大专院校师生、科研院所及企业的研究人员和技术人员。 Member of Chinese Society of Particuology, and researchers or experts who are engaged in the study of particle sciences and technology coming from colleges, institutes and corporations all over the world.
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    Morphology of impact fragmentation distribution of single spherical and ellipsoidal particles in drop weight experiments

    Qiuhua MiaoPeng HuangWenchang Zhu
    137-148页
    查看更多>>摘要：Particle shape is an important factor affecting the fragmentation distribution of the ore particles.To investigate the influence of particle shape on the morphological fragmentation distribution character-istics,the crushable ore particles are defined as prolate,oblate ellipsoid and spherical particles,which have different aspect ratios(AR)and sphericity(S).Based on the drop weight experiment,the influence of the net drop height on the macroscopic mechanical behavior and crushing distribution characteristics of the single spherical and ellipsoidal particles is studied.The results show that different peak-shifting characteristics exist during particle fragmentation.The fragmentation distribution peak shifts left when the increased impact energy is eventually only enough to break medium-sized sub-particles.Conversely,it shifts right when impact energy is increased enough to break largest-sized sub-particles.Besides,regardless of whether the net drop height changes,the maximum continuous fragmentation degree presents"M"-shaped characteristic with the increased AR.Compared with the ellipsoid particles,the single spherical particle is more difficult to be broken by impact,with wider equivalent particle fragmentation distribution.With the increase of particle sphericity,the maximum continuous frag-mentation degree of a single ellipsoid particle has an overall trend of initial increase and subsequent decrease.Especially when particle sphericity is 0.9＜S＜0.95,the maximum continuous fragmentation degree of both prolate and oblate ellipsoid particles is much higher.
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    Accurate characterization of bubble mixing uniformity in a circular region using computational geometric theory

    Hui SunJianxin XuShibo WangGuangcheng Cai...
    149-159页
    查看更多>>摘要：The present study proposes a novel method based on the geometric theory for measuring the distri-bution of bubble swarms in the circular region of a direct-contact heat exchanger.It was determined that the mixing is uniform when the average distance between the bubble swarms in the unit circular region is approximately 0.9054,which is the standard reference value.The effect of sample size(i.e.,the number of bubbles)on mixing uniformity was investigated to determine the optimal sample size.It was verified that the metric's accuracy and stability were higher with a sample size of 155.Accordingly,it was proposed to increase the sample size by filling irregular bubbles using a segmentation method,which enabled a further accurate assessment of the mixing uniformity.The mixing uniformity of bubble swarms in the circular region and its maximum internal connection with the square region was accu-rately quantified.It was revealed that the relative average error increased by approximately 3.47％due to information loss.The proposed method was demonstrated to be rotationally invariant.The present study provided novel insights into evaluating mixing uniformity,which would guide enhanced heat transfer and the effective evaluation of the spatiotemporal characteristics of transient mixing in circular regions or the cross-sections of chemical transport pipelines.
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    Electrode particulate materials for advanced rechargeable batteries:A review

    Mingyang MaMiao DuYan LiuHongyan Lü...
    160-181页
    查看更多>>摘要：The demand for large-scale energy storage is increasing due to the decreasing non-renewable resources and deteriorating environmental pollution.Developing rechargeable batteries with high energy density and long cycle performance is an ideal choice to meet the demand of energy storage system.The development of excellent electrode particles is of great significance in the commercialization of next-generation batteries.The ideal electrode particles should balance raw material reserves,electro-chemical performance,price and environmental protection.Among them,the development of electrode particulate materials with excellent electrochemical properties is the top priority at present.In this re-view,the typical researches of electrode materials are summarized in terms of crystal structure,morphology,pore structure,surface and interface regulation.Firstly,the structural characteristics and improvement methods of transition metal oxides,polyanionic compounds,Prussian blue and their an-alogues are introduced.Then,the different effects of particulate morphology,pore,surface and interface structure on the performance of electrode materials are discussed.For designing high-performance electrode materials,preparation route should be set according to the particle properties of the mate-rials and the synergistic effect of various optimization methods should be adopted.At the same time,in addition to the electrode materials,other components of the rechargeable batteries,such as current collector,separator and electrolytes,should be optimized to improve the overall performance of the batteries.This review would provide important guiding principle for designing high-performance electrode particulate materials.
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    Evolution of biomass particles during pelletization process

    Hamid RezaeiMaryam TajilrouJun Sian LeeKanages Singaraveloo...
    182-187页
    查看更多>>摘要：Pulverizing is an essential unit operation in co-firing biomass with coal.Pulverizers are only compatible with pellet forms of fibrous biomass materials and crush them down to their original forming particle sizes.That is why the data on the size distribution of the particles forming a biomass pellet is crucial to achieving optimum combustion conditions.The current study determines the internal particle size distribution of pellets after wet disintegration,following ISO 17830 standard,and aims to suggest im-provements to the mentioned standard based on new measured evidence.Experiments were carried out on white wood pellets(no bark)and brown wood pellets containing bark at four water temperatures:20,40,60,and 95 ℃,with or without stirring.The particle size distribution of the pre-pelletizer wood particles was also measured and compared with particles in the formed pellets.Ambient water tem-perature of 20 ℃ was found to be adequate for the complete disintegration of pellets,and no mechanical stirring was required.About 30％of particles in the disintegrated pellets were 0.5-1.0 mm.Pelletization changes the particle size distribution to smaller particles.The disintegrated bark pellets contained more fines than white pellets.
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    Hydrodynamics and OCM reaction performance in a bubbling fluidized bed reactor and a riser reactor

    Min CaiShuangzhu KongSheng ChenMengxi Liu...
    188-204页
    查看更多>>摘要：The reasonable reactor design is of great importance for increasing the C2 yield(C2H4 and C2H6)of the oxidative coupling of methane(OCM),and the OCM reactor should remove the heat released in reactions quickly and efficiently and minimize the consecutive reaction of ethylene to carbon oxides.The fluidized bed reactor is characterized by excellent heat transfer,superior mass transport,and large handling ca-pacity,while fewer studies focused on large-scale fluidized bed reactors for the OCM reaction.Therefore,large cold-model experiments and computational fluid dynamics simulations were conducted to investigate hydrodynamics and the OCM reaction performance in a large-scale bubbling fluidized bed(BFB)and a large-scale riser.In the BFB reactor,consecutive reactions of ethylene are acute because of the strong gas back-mixing,high solids holdup,and non-uniform solids distribution.While the consecutive reactions of ethylene are negligible due to the plug flow structure and low solids holdup in the riser reactor.Further,both reactors can achieve isothermal operation for the OCM process.The C2 selectivity of 45.4％and C2 yield of 21.1％are obtained in the riser reactor,increasing by 20.3％and 5.8％individually than that in the BFB reactor.This study provides useful information and reference to the OCM reactor design and commercialization.
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    Construction and properties of venlafaxine hydrochloride sustained release system based on hollow mesoporous silica microspheres

    Chenjing LiangLingling ShiZhengguo ChenLan Zhou...
    205-210页
    查看更多>>摘要：The aim of this work is to develop a venlafaxine hydrochloride sustained release system based on hollow mesoporous silica microspheres(HMSMs).HMSMs were innovatively prepared with tetraethyl silicate(TEOS)as the precursor and volatile n-heptane as a soft template.The obtained HMSMs show a well-defined hollow structure with an average size of 967 nm and pore volume of 0.85 cm3/g,implying it is a potential drug carrier.Subsequently,venlafaxine hydrochloride(VF)was absorbed in the HMSMs with a content of 37.67％or so.The sustained release effect is further measured by the dissolution in-strument at 37 ℃ and 50 rpm in ultrapure water.The results showed that the HMSMs/VF system shows good sustained release properties compared with sustained release tablets with hydroxypropyl meth-ylcellulose as the main component.This HMSMs sustained release system appears to be a promising candidate for a sustained drug release.
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    Modelling the formation and dissolution behavior of alumina agglomerate in the cryolite

    Jiaqi WangMao LiBenjun ChengHesong Li...
    211-222页
    查看更多>>摘要：The presence of alumina agglomerates seriously affects the current efficiency of the aluminum elec-trolysis process.Clarify the dynamic dissolution process of agglomerates is essential to improve the current efficiency of aluminum electrolysis.A mathematical model is proposed to describe the different phenomena from the formation until complete dissolution of agglomerates.Considering permeation and solidification processes of cryolite,a semi-analytical mathematical model is developed to formulate the formation,melting and dissolution processes of agglomerates,and the time duration for each stage is deduced.Porosity and heat mass transfer of agglomerates are explored based on the packing theory and mechanism of heat mass transfer in wet porous media.Dimensionless approach is applied to investigate the main factors affecting the dissolution stages and porosity of agglomerates.The results show that the superheat has a great influence on the formation and melting stage,the diameter of agglomerates can reach 14.93 mm for 200 particles agglomerated.The density decreases with the increase of agglomerated particle number,which varies in the range of 2.27-2.28 g/cm3.The average dissolution rate of ag-glomerates is about 1.83 x 10-5-2.95 x 10-5 kg/s within the range of alumina concentration in this study.
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    Bubble dynamics properties of B-particles in a quasi-2D gas-solid fluidized bed:Computational particle fluid dynamics numerical simulation and post-processed by digital image analysis technique

    Zemin YuanZhong HuangGuotao QinGuanjia Zhao...
    223-238页
    查看更多>>摘要：Bubble dynamics properties play a crucial and significant role in the design and optimization of gas-solid fluidized beds.In this study,the bubble dynamics properties of four B-particles were investigated in a quasi-two-dimensional(quasi-2D)fluidized bed,including bubble equivalent diameter,bubble size distribution,average bubble density,bubble aspect ratio,bubble hold-up,bed expansion ratio,bubble radial position,and bubble velocity.The studies were performed by computational particle fluid dy-namics(CPFD)numerical simulation and post-processed with digital image analysis(DIA)technique,at superficial gas velocities ranging from 2umf to 7umf.The simulated results shown that the CPFD simu-lation combining with DIA technique post-processing could be used as a reliable method for simulating bubble dynamics properties in quasi-2D gas-solid fluidized beds.However,it seemed not desirable for the simulation of bubble motion near the air distributor at higher superficial gas velocity from the simulated average bubble density distribution.The superficial gas velocity significantly affected the bubble equivalent diameter and evolution,while it had little influence on bubble size distribution and bubble aspect ratio distribution for the same particles.Both time-averaged bubble hold-up and bed expansion ratio increased with the increase of superficial gas velocity.Two core-annular flow structures could be found in the fluidized bed for all cases.The average bubble rising velocity increased with the increasing bubble equivalent diameter.For bubble lateral movement,the smaller bubbles might be more susceptible,and superficial gas velocity had a little influence on the absolute lateral velocity of bubbles.The simulated results presented a valuable and novel approach for studying bubble dynamics properties.The comprehensive understanding of bubble dynamics behaviors in quasi-2D gas-solid fluidized beds would provide support in the design,operation,and optimization of gas-solid fluidized bed reactors.
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    NeuroPNM:Model reduction of pore network models using neural networks

    Robert JendersieAli MjalledXiang LuLucas Reineking...
    239-251页
    查看更多>>摘要：Reacting particle systems play an important role in many industrial applications,for example biomass drying or the manufacturing of pharmaceuticals.The numerical modeling and simulation of such sys-tems is therefore of great importance for an efficient,reliable,and environmentally sustainable operation of the processes.The complex thermodynamical,chemical,and flow processes that take place in the particles are a particular challenge in a simulation.Furthermore,typically a large number of particles is involved,rendering an explicit treatment of individual ones impossible in a reactor-level simulation.One approach for overcoming this challenge is to compute effective,physical parameters from single-particle,high-resolution simulations.This can be combined with model reduction methods if the dynamical behaviour of particles must be captured.Pore network models with their unrivaled resolution have thereby been used successfully as high-resolution models,for instance to obtain the macroscopic diffusion coefficient of drying.Both parameter identification and model reduction have recently gained new impetus by the dramatic progress made in machine learning in the last decade.We report results on the use of neural networks for parameter identification and model reduction based on three-dimensional pore network models(PNM).We believe that our results provide a powerful complement to existing methodologies for reactor-level simulations with many thermally-thick particles.
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    A novel method for modeling the phase change of iron ore particles in the cohesive zone of a blast furnace

    Dianyu EYingming WenJiayun DanYouyuan Jiang...
    252-261页
    查看更多>>摘要：Cohesive zone plays a vital role in the stable operation of a blast furnace(BF),yet the complex phase change process of iron ore particles in this zone is still not well understood.In this study,a novel one-dimensional(1D)unsteady phase change model was developed to elucidate the heat transfer and melting mechanisms of iron ore particles.After model validation,the effects of several key operating parameters(e.g.,particle diameter,gas velocity,initial temperature)on the phase change behavior of iron ore particles were analyzed,and the joint effect of multiple parameters was discussed.The results show that larger-sized iron ore particles possess lower specific surface areas,which in turn reduces their convective heat absorption capacity.Consequently,the distance from the solid-liquid phase interface to the particle surface increases,thereby slowing down the movement of the phase interface and pro-longing the melting duration of the particles.Increasing the gas velocity and the initial temperature does not have a significant impact on reducing the duration of the complete melting process.Under the specified conditions,it is observed that increasing the gas velocity by 3-fold and 9-fold results in a reduction of the melting duration by 2.4％and 8.3％,respectively.Elevating the initial temperature of iron ore particles results in a decrease in the core-to-surface temperature difference,a slower heating rate,and a shorter duration to achieve melting.Among the factors affecting the melting process,the particle diameter is found to be the most significant in terms of the liquid phase precipitation,mushy zone thickness,and core-to-surface temperature difference of iron ore particles.
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