多孔结构Ti3SiC2材料的制备工艺研究
Study on Preparation Technology of Porous Ti2SiC2 Materials
王佳杰 1杨李林 1李陈 1郑浩 1黄晓晨1
作者信息
- 1. 蚌埠学院材料与化学工程学院,安徽蚌埠 233030
- 折叠
摘要
以Ti3SiC2粉末为原料,聚乙烯亚胺为分散剂,去离子水为分散介质,聚氨酯海绵为多孔模板,系统地研究了分散剂对浆料pH的影响以及pH对Ti3SiC2水基浆料稳定性的影响.采用有机浸渍法制备多孔Ti3SiC2预制体,对多孔Ti3SiC2材料孔隙率和物相进行分析,可知水基浆料中含质量分数为30％的Ti3SiC2样品的性能最佳,其总孔隙率为66％,比表面积为90％,材料以闭口型小孔为主.
Abstract
Using Ti3SiC2 powder as raw material,polyethyleneimine as dispersant,deionized water as dispersion medium,and polyurethane sponge as porous template,the influence of dispersant on pH of slurry and the influence of pH on stability of Ti3SiC2 water-based slurry were systematically studied.Porous Ti3SiC2 preforms were prepared by organic impregnation method.Porosity and phase analysis of porous Ti3SiC2 materials were carried out.When the mass fraction of Ti3SiC2 sample in water-based slurry was 30％,the performance was the best.Its total porosity is 66％,specific surface area is 90％,and the material is mainly closed pores.
关键词
Ti3SiC2/多孔/孔隙率Key words
Ti3SiC2/porous/porosity引用本文复制引用
基金项目
国家级大学生创新创业训练计划(202111305001)
国家级大学生创新创业训练计划(202111305005)
省级大学生创新创业训练计划(S202111305006)
煤清洁转化与高值化利用安徽省重点实验室开放基金(CHV19-05)
安徽省科学研究重大项目(KJ2021ZD0141)
安徽省自然科学基金面上项目(2208085ME104)
出版年
2024
NETL
NSTL
万方数据