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马齿苋中总酚提取工艺研究

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以马齿苋为原料,选取超声波辅助法对其中的总酚进行提取测定.通过单因素实验探究了超声时间、乙醇浓度、超声温度、料液比对多酚得率的影响.在单因素实验基础上,结合响应面分析法优化提取工艺.实验表明:超声时间为114 min,提取温度为66℃,料液比为1∶28(g/mL),乙醇体积分数为34%时,多酚得率最高,为44.02%.
Study on Extraction Process Technology of Total Phenols from Purslane
In this study,the total phenols in purslane were extracted by ultrasonic-assisted method.The extraction time,the ethanol concentration,the extraction temperature and the feed-to-liquid ratio were investigated by single fac-tor experiment according to absorbance of the total phenols in purslane.Based on the single factor experiments,the ex-traction technology was optimized by response surface test.The analysis of the experimental data showed that the extrac-tion time was 114 min,extraction temperatureand was 66℃,the feed-to-liquid ratio was 1∶28(g/mL),and the volume-fraction of ethanol was 34%,the extraction rate of total phenols reached the highest,was 44.02%.

purslanetotal phenolsultrasonic extractionresponse surface testextraction process technology

曹利慧、肖梓莹、曹作佳、李胜杰、高兢

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衡水学院应用化学系,河北衡水 053000

马齿苋 总酚 超声波 响应面分析法 提取工艺

衡水学院省级大学生创新创业训练计划衡水学院校级项目

S2022101010062023ZRZ06

2024

安徽化工
安徽省化工研究院

安徽化工

影响因子:0.229
ISSN:1008-553X
年,卷(期):2024.50(1)
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