首页|β-环糊精碳材料吸附处理苯酚污水的研究

β-环糊精碳材料吸附处理苯酚污水的研究

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采用β-环糊精作为原料,磷酸为活化剂制备β-环糊精碳材料,考查了单因素条件(活化温度、活化时间、浸渍比)对制备的碳材料产品性能的影响,得到了磷酸活化法制备活性炭的最佳工艺条件,即浸渍比为1∶2,时间为3 h,温度为500℃,测定最佳工艺条件下β-环糊精碳材料对苯酚溶液的吸附性能,考查了单因素条件(初始浓度、吸附时间、投炭量)对碳材料吸附苯酚的影响,得到了 β-环糊精碳材料吸附苯酚的三个最佳优化条件,即苯酚溶液初始浓度40 mg·L-1,吸附时间30 min,投碳量0.09 g.磷酸活化法制备β-环糊精碳材料的工艺过程及其吸附性能的研究,为苯酚污水的预处理和实现水资源的循环利用有一定的借鉴意义.
Adsorption Treatment of Phenol Wastewater by β-Cyclodextrin Carbon Material
The[3-cyclodextrin carbon materials were prepared by using[3-cyclodextrin as the raw material and phosphoric acid as the activator.The effects of single-factor conditions(activation temperature,activation time,and impregnation ra-tio)on the product properties of the prepared carbon materials were investigated.The optimal process conditions for the preparation of activated carbon by the phosphoric acid activation method were obtained,i.e.,the impregnation ratio of 1∶2,the time of 3 h,and the temperature of 500℃.The carbon material was adsorbed to the phenol solution under the optimal process conditions.The adsorption performance of β-cyclodextrin carbon materials on phenol solution under the optimal process conditions was determined,and the effects of one-factor conditions(initial concentration,adsorption time,and amount of carbon injected)on the adsorption of phenol by the carbon materials were investigated,and three optimal optimi-zation conditions for the adsorption of phenol by β-cyclodextrin carbon materials were obtained,i.e,an initial concentra-tion of 40 mg·L-1 of phenol solution,an adsorption time of 30 min,and an amount of carbon injected of 0.09 g.Phosphoric acid activation method for the process of preparing β-cyclodextrin carbon material and its adsorption performance can be a practical reference for the pretreatment of phenol wastewater to realize the recycling of water resources.

β-cyclodextrincarbon materialsadsorption performancephenol effluent

徐世洁、胡志泉、沈国良、薛丽丽

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沈阳工业大学石油化工学院,辽宁辽阳 111003

β-环糊精 碳材料 吸附性能 苯酚污水

2024

安徽化工
安徽省化工研究院

安徽化工

影响因子:0.229
ISSN:1008-553X
年,卷(期):2024.50(3)