首页|脉冲激光熔覆Inconel 718涂层热行为数值模拟及其对显微组织的影响

脉冲激光熔覆Inconel 718涂层热行为数值模拟及其对显微组织的影响

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目的 揭示脉冲激光作用下Inconel 718合金涂层凝固传热行为的演化机制,改善涂层中Nb、Mo元素偏析现象,提升Inconel 718合金熔覆涂层的力学性能,为优化Inconel 718熔覆涂层质量提供理论依据.方法 综合考虑物性参数随温度、脉冲激光热源、粉末传输形式,以及凝固过程中相变潜热对涂层凝固热行为的影响,构建脉冲激光熔覆传热模型.基于数值模拟技术和激光熔覆试验,利用VHX-2000电子显微镜对涂层显微组织形态进行分析验证,采用日立SU8010场发式扫描电镜观察分析显微组织和元素偏析情况,并使用显微硬度计测试涂层的硬度值.结果 由数值模拟分析结果可知,脉冲激光涂层的冷却速度、温度梯度、凝固速度均大于连续激光涂层,其枝晶生长细密且No、Mo元素呈弥散分布,显微组织自底向顶以平面晶、胞状枝晶、柱状枝晶、等轴枝晶等形式存在,Laves相的体积分数降低至2.93%,在细晶强化和固溶强化作用下,熔覆涂层的平均显微硬度提升至307HV0.1.结论 脉冲激光涂层热行为数值模拟分析结果符合Inconel 718涂层组织形态快速凝固变化的规律,数值模型可靠.脉冲激光形成的高冷却速度和高温度梯度,能在一定程度上抑制Inconel 718合金涂层中Nb、Mo元素的偏析,离散并细化γ 枝晶组织,降低Laves相的体积分数,显微组织在细晶强化和固溶强化双重作用下,提升涂层的力学性能.
Numerical Simulation of Thermal Behavior of Inconel 718 Coating Prepared by Pulsed Laser Cladding and Its Effect on Microstructure
As a new green and environment-friendly material preparation technology, laser cladding technology expands the use of Inconel 718 alloy materials, but the non-equilibrium solidification process of cladding pool is often accompanied by the segregation of elements such as Nb and Mo, finally forming Laves phase. At the same time, the high-heat laser input is easy to coarsen the dendritic structure and reduce the mechanical properties of the coating. For this reason, the work aims to investigate the evolution mechanism of solidification heat transfer behavior of Inconel 718 alloy coating under pulsed laser to explore the effects of pulsed laser on element segregation, microstructure and mechanical properties of the coating, so as to provide a theoretical basis for optimizing the quality of Inconel 718 cladding coating.The effects of physical parameters with temperature, pulsed laser heat source, powder transmission form and phase transformation latent heat during solidification on the solidification thermal behavior of the coating were comprehensively considered, and the heat transfer model of pulsed laser cladding was established. Laser cladding experiments were carried out by a fiber laser (wavelength 1070 nm and spot diameter 3 mm) and a six-degree-of-freedom series manipulator. After the test, the WEDM equipment was used to prepare the specimen along the longitudinal and transverse direction of the cladding layer. After polishing, the specimen was etched by Kalling's 2 etching agent (5 g CuCl2+100 mL HCl+100 mL C2H5OH) for 10 seconds. The microstructure and morphology of the coating were analyzed by VHX-2000 electron microscope, and the reliability of the numerical model was verified. The phase analysis of the pulsed laser coating was carried out by a diffractometer (D8/advance) at a scanning speed of 2 (°)/min and a diffraction angle of 10°-80°. The hardness of the coating prepared by two laser modes was tested by microhardness tester (DUH-211) (test load 1000 mN, material Poisson's ratio 0.3 and maintenance time 10 s), and the effect of pulsed laser on the microstructure and mechanical properties of Inconel 718 coating was investigated.The numerical simulation results showed that the cooling rate, temperature gradient and solidification rate of pulsed laser coating were higher than that of CW laser coating, the dendrite growth of pulsed laser coating was fine and the elements of No and Mo were dispersed. The microstructure existed in the form of plane crystal, cellular dendrite, columnar dendrite and equiaxed dendrite from bottom to top. The volume fraction of Laves phase in the coating was reduced to 2.93%. Under the action of fine grain strengthening and solid solution strengthening, the average microhardness of the coating increased to 307HV0.1.The numerical simulation results of thermal behavior of pulsed laser coating are consistent with the law of rapid solidification of Inconel 718 coating. The numerical model is reliable. The high cooling rate and high temperature gradient formed by pulsed laser can inhibit the segregation of Nb and Mo elements in Inconel 718 alloy coating, disperse and refine γ dendrite structure, and reduce the volume fraction of Laves phase. The microstructure improves the mechanical properties of the coating under the action of fine grain strengthening and solid solution strengthening.

laser claddingInconel 718pulsed lasernumerical simulationmicrostructure and properties

吴军、蔡建臣、王胜、李董航、周寒文

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衢州学院,浙江 衢州 324000

浙江省空气动力装备技术重点实验室,浙江 衢州 324000

衢州职业技术学院,浙江 衢州 324000

激光熔覆 Inconel 718 脉冲激光 数值模拟 组织性能

浙江省基础公益研究计划项目浙江省基础公益研究计划项目

LTGC23E050001LGC21E050002

2024

表面技术
中国兵器工业第五九研究所,中国兵工学会防腐包装分会,中国兵器工业防腐包装情报网

表面技术

CSTPCD北大核心
影响因子:1.39
ISSN:1001-3660
年,卷(期):2024.53(11)
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