传感器与微系统2024,Vol.43Issue(4) :17-20.DOI:10.13873/J.1000-9787(2024)04-0017-04

基于微孔封装氧化镍的CO敏感材料性能研究

Study on characteristics of CO-sensitive materials based on microporous encapsulated nickel oxide

王博 葛江亚 刘继江 王烜赫 高云鹏 胡宇涵
传感器与微系统2024,Vol.43Issue(4) :17-20.DOI:10.13873/J.1000-9787(2024)04-0017-04

基于微孔封装氧化镍的CO敏感材料性能研究

Study on characteristics of CO-sensitive materials based on microporous encapsulated nickel oxide

王博 1葛江亚 2刘继江 1王烜赫 1高云鹏 1胡宇涵1
扫码查看

作者信息

  • 1. 中国电子科技集团公司第四十九研究所,黑龙江哈尔滨 150028
  • 2. 中国航天员科研训练中心,北京 100094
  • 折叠

摘要

一氧化碳(CO)是在生活、生产中常见的可燃性气体,对人体伤害巨大.因此,实现CO的高灵敏、高稳定检测具有重要意义.采用牺牲模板法与等体积浸渍相结合的方式制备出NiO@MGC新型复合敏感材料.通过XRD,BET,SEM,TEM表征方法对不同负载量样品形貌、晶体结构进行表征.证明了制备的复合材料继承了分子筛模板的微孔结构,并且NiO均匀限域在微孔孔道中.制作成传感器探头进行气敏性能测试,结果表明:传感器可以实现对CO在10 ×10-6~50 ×10-6范围内的快速检测,并且具有良好的稳定性.同时验证了传感器在NO2,NH3和乙醇的干扰下可以实现CO选择性检测.

Abstract

Carbon monoxide(CO)is a common flammable gas in life and production,which is very harmful to the human body.Therefore,it is of great significance to realize the high sensitivity and high stability detection of CO.A new type of composite sensitive material NiO@MGC is prepared by combining the sacrificial template method with the equal volume impregnation.The morphology and crystal structure of the samples with different loadings are characterized by XRD,BET,SEM and TEM.It is proved that the prepared composite material inherites the microporous structure of the molecular sieve template,and NiO is uniformly confined in the microporous channels.Sensor probe is made for gas sensitivity test.The results show that the sensor can realize the rapid detection of CO in the range of10×10-6~50 ×10-6,and has good stability.At the same time,it is verified that the sensor can realize selective detection of CO under the interference of NO2,NH3 and ethanol.

关键词

类石墨烯碳/氧化镍/一氧化碳传感器

Key words

graphene like carbon/NiO/CO sensor

引用本文复制引用

出版年

2024
传感器与微系统
中国电子科技集团公司第四十九研究所

传感器与微系统

CSTPCD北大核心
影响因子:0.61
ISSN:1000-9787
参考文献量10
段落导航相关论文