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高一致性全固态水下电场传感器的制备与性能测量

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本文综合国内外的电极制备的设计工艺和结构,利用固相球磨加冷冻干燥制备全固态Ag/AgCl电极前驱粉体,在与纳米银粉混合中添加碳纳米管(CNTs)作为造孔剂,经压制烧结得到Ag/AgCl电极坯体.设计了内置电极溶液的结构,解决了电极裸露在海水中不稳定和存储运输困难的问题.使用DM6500六位半万用表和EMA10斩波放大器为核心的测量平台对电极性能进行了测量,所设计制备的6个电极,任意电极配对极差最大约38μV,电极对漂移小于5μV/24 h,电极自噪声小于0.7 nV/√Hz@1 Hz.所设计制备的水下电场传感器达到了国内外先进水平,且具备了工程化应用能力.
Preparation and performance measurement of high-consistency all-solid-state underwater electric field sensor
Design processes and structures of domestic and international electrode preparation are integrated,utilizing solid-phase ball milling and freeze-drying to prepare all-solid Ag/AgCl electrode precursor powder.Carbon nanotubes(CNTs)are added as a pore-forming agent during the mixing with nano-silver powder,and the Ag/AgCl electrode blanks are obtained through pressing and sintering. A structure with an built-in electrode solution is designed,addressing issues of electrode instability when exposed to seawater and difficulties in storage and transportation. The electrode performance are measured using a measurement platform centered around a DM6500 six-and-a-half digital multimeter and an EMA10 chopper amplifier. Among the designed and prepared six electrodes,the maximum difference between any electrode pairs is about 38μV,the electrode pair drift is less than 5μV/24 h,and the electrode self-noise is less than 0. 7 nV/√Hz@1 Hz. The designed and prepared underwater electric field sensor reaches the advanced level both domestically and internationally,and possesses engineering application capabilities.

electric field sensorAg/AgCl electrodedriftself-noise

张扬、牛晓博、姚琦、纪延达

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海军士官学校信息通信系,安徽 蚌埠 233012

电场传感器 Ag/AgCl电极 漂移 自噪声

2024

传感器与微系统
中国电子科技集团公司第四十九研究所

传感器与微系统

CSTPCD北大核心
影响因子:0.61
ISSN:1000-9787
年,卷(期):2024.43(7)
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