材料导报2025,Vol.39Issue(1) :281-285.DOI:10.11896/cldb.23090126

超高真空环境下TC4钛合金和ZrO2陶瓷的出气性能研究

Research on the Outgassing Performance of TC4 Titanium Alloy and ZrO2 Ceramics Under Ultra-high Vacuum

焦纪强 蒙峻 谢文君 刘建龙 魏宁斐 罗成 郭方准 王润成
材料导报2025,Vol.39Issue(1) :281-285.DOI:10.11896/cldb.23090126

超高真空环境下TC4钛合金和ZrO2陶瓷的出气性能研究

Research on the Outgassing Performance of TC4 Titanium Alloy and ZrO2 Ceramics Under Ultra-high Vacuum

焦纪强 1蒙峻 2谢文君 3刘建龙 2魏宁斐 3罗成 3郭方准 4王润成4
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作者信息

  • 1. 大连交通大学机械工程学院,辽宁大连 116000;中国科学院近代物理研究所,兰州 730000
  • 2. 中国科学院近代物理研究所,兰州 730000;中国科学院大学核科学与技术学院,北京 100049
  • 3. 中国科学院近代物理研究所,兰州 730000
  • 4. 大连交通大学机械工程学院,辽宁大连 116000
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摘要

内衬超薄壁真空腔体是离子加速器真空系统的核心元件,为了获得超高真空环境,对内衬材料的出气性能有较高要求.基于新型双通道出气率实验装置,完成了 TC4钛合金和ZrO2陶瓷在常温抽气、不同烘烤温度及烘烤结束后不同温度下的出气率实验;通过数值拟合方法获得了材料在不同加热温度下的出气率表达式;搭建了钛合金内衬超薄壁真空腔体压力实验装置,通过实验和仿真对比分析了不同工况下的压力分布.结果表明,烘烤温度越高,最终出气率越低,250 ℃烘烤时出气率较150℃时降低了约21%.经过高温烘烤后,当材料温度从50℃升高至210℃时,两种材料的出气率呈指数增加趋势,但钛合金的出气率低于陶瓷的出气率.常温抽气和烘烤过程中真空腔体压力梯度较小,对其进行升温时中间位置压力变化幅度较大,当温度为100 ℃,中间位置压力从初始值1.41x10-9 Pa升高至4.51x10-9 Pa;压力仿真结果和实验结果一致,平均相对偏差为6.86%.以上结果填补了钛合金和陶瓷出气率数据库,能够预测及评估真空腔体不同工况下的极限压力,为超高、极高真空获取提供数据支撑.

Abstract

The inner lined thin-walled vacuum chamber is the core of ion accelerator vacuum system.In order to obtain ultra-high vacuum,there is a high requirement for the outgassing performance of the inner material.Based on a new dual channel outgassing rate test system,the outgassing rate of TC4 titanium alloy and ZrO2 ceramics were completed at room temperature pumping,different baking temperatures and different heating temperatures after baking.The mathematical expressions of outgassing rate at different temperatures were obtained by fitting method.The pres-sure test system of titanium alloy lined chamber was developed,and the pressure distribution under different conditions was obtained by experi-ment and simulation.The result showed that the higher baking temperature,the lower ultimate outgassing rate.Compared to the baking tempera-ture of 150 C,the outgassing rates of alloy and ceramics decreased by 21%at the baking temperature of 250 ℃.After baking,at the tempera-ture between 50 ℃ and 210 ℃,the outgassing rate of the two materials showed an exponentially increasing trend,but the outgassing rate of tita-nium alloy was lower than that of ceramics.Besides,the chamber pressure gradient was relatively smooth in the process of room temperature and baking,but the pressure at the middle position changed greatly under different heating temperatures.When the temperature increased from room temperature to 100 ℃,the middle position pressure increased from 1.41×10-9 Pa to 4.51 ×10-9 Pa.The simulation results were consistent with the experimental results,and the average relative deviation was 6.86%.The above results should fill the outgassing rate database of titanium alloy and ceramics,which could be helpful to predict and evaluate the ultimate pressure of the inner lined thin-walled vacuum chamber under dif-ferent working conditions,and provide support for ultra-high vacuum and extremely high vacuum acquisitions.

关键词

离子加速器/超高真空/TC4钛合金/ZrO2陶瓷/出气率/压力分布

Key words

ion accelerator/ultra-high vacuum/TC4 titanium alloy/ZrO2 ceramic/outgassing rate/pressure distribution

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出版年

2025
材料导报
重庆西南信息有限公司

材料导报

CSCD北大核心
影响因子:0.605
ISSN:1005-023X
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