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主动钻杆接头金属复合陶瓷渗镀表面强化技术研究

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为提高主动钻杆接头表面硬度、耐磨性等各项力学性能,采用熔盐法,以TiO2粉末为原料,在氮气气氛下,将TiO2粉末置于NaCl-MgCl2熔盐中并加入微量Ag、Cu粉末,在500~800℃下反应16 h得到接头表面梯度氮化物陶瓷相.对强化后的接头进行表面硬度、显微组织及物相和耐磨性能等的测试和分析,结果表明,渗镀层形成了TiN及FexTi(Ag,Cu)强化相;表面硬度提高到1 710HV0.05;比磨损率下降到0.027 0 mm3/(N·m);耐磨性比常规氮化的提高了 1.8倍,比基体材料的提高了 6.8倍.这表明与常规氮化工艺相比,金属复合陶瓷渗镀工艺可在强化表面形成多梯度渗镀层结构,具备减磨、降温、自润滑的效果,能极大提高接头表面硬度及耐磨性等各项力学性能.
Study on Surface Hardening Technology of Metal Composite Ceramic Alloying Plating for Active Drill Pipe Joint
TiO2 powders are placed in NaCl-MgCl2 molten salt with tiny amount of Ag and Cu powders at 500-800 ℃ for 16 hours to prepare the gradient nitride ceramic phase on the surface of active drill pipe joint,therefore to improve the adhesion re-sistance,wear resistance and mechanical properties of the joint.The hardness,microstructure,phase and wear resistance of the strengthened joint are tested and analyzed.It is found out that strengthening phases of TiN and FexTi(Ag,Cu)are formed in the infiltration layer.The surface hardness increases to 1 710HV0.05,the specific wear rate decreases to 0.027 0 mm3/(N·m),and the wear resistance is 1.8 times higher than that of the ordinary nitrided joint,and 6.8 times higher than that of the matrix material.Compared with the common surface nitriding process,the composite cermet infiltration process forms a multi-gradient infiltration coating structure on surface of the joint,which has the effects of reducing wear,cooling and self-lubrication,and can greatly improve the surface hardness and wear resistance of the active drill pipe joint.

active drill pipe jointcomposite cermet infiltration platingsurface hardnesswear rate

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中煤科工集团西安研究院有限公司,陕西西安 710077

主动钻杆接头 金属复合陶瓷渗镀 表面硬度 磨损率

陕西省自然科学基础研究计划陕西省自然科学基础研究计划2023年度中煤西安研究院科技创新基金项目

2021JQ-9502021JQ-9512023XAYJS27

2024

材料开发与应用
洛阳船舶材料研究所 中国造船工程学会船舶材料学术委员会

材料开发与应用

CSTPCD
影响因子:0.342
ISSN:1003-1545
年,卷(期):2024.39(3)