首页|TB9钛合金棒线材制备过程中微观组织和力学性能演变

TB9钛合金棒线材制备过程中微观组织和力学性能演变

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通过光学显微镜、扫描电镜、电子背散射衍射技术等系统研究了 TB9钛合金棒线材在制备过程中的微观组织及力学性能的演变过程.结果表明:通过真空自耗电弧熔炼、锻造、轧制及拉拔等工艺能够制备出表面质量良好、横截面组织性能一致的不同规格TB9钛合金棒线材产品.其中,开坯锻态组织由随机取向的粗大β相及极少量动态再结晶(DRX)晶粒构成,平均晶粒尺寸在1 000 µm以上.径锻态组织主要由约400 µm的β晶粒构成,累计应变的增加使得DRX晶粒百分数增加.多道次热变形获得的φ10 mm棒材盘圆组织由尺寸为15 μm的细小晶粒组成,具有显著的热加工变形特征,固溶水冷处理能使组织均匀并获得无畸变β晶粒.热拉拔变形能够进一步细化晶粒,并提高TB9钛合金强度,强度最高可达1 100 MPa以上,但塑性有所下降.
Evolution of Microstructure and Mechanical Properties of TB9 Alloy Bar and Wire during Production Process
The evolution of microstructures and mechanical properties of TB9 titanium alloy bar and wire during the production process is systematically studied by means of optical microscope,scanning electron microscope and electron backscattered dif-fraction.The results show that the TB9 titanium alloy bar and wire with good surface quality,consistent cross-section micro-structures and properties can be prepared by vacuum consumable arc melting,forging,rolling and drawing.The as-forged mi-crostructure is composed of randomly oriented coarse β grains and very few dynamic recrystallization(DRX)grains,with an aver-age grain size of more than 1 000 μm.The radial forged microstructure is mainly composed of β grains with the size of about 400μm,and the increase of cumulative deformation increases the DRX fraction.The microstructure of φ10 mm wire rod obtained by multi-pass hot deformation is composed of fine grains of 15 µm,which has obvious hot deformation characteristics.Compared with air cooling,the water cooling of solid solution treatment can obviously uniform the microstructure and obtain distortionless βgrains.The hot drawing deformation can further refine the grains and improve the strength of TB9 titanium alloy up to more than 1 100 MPa,while reduces the plasticity.

TB9 titanium alloybar and wiremicrostructuremechanical propertiesdynamic recrystallization

董恩涛、滕艾均、耿乃涛、方强、康强、郭杰、张天馨

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鞍钢集团北京研究院有限公司,北京 102211

成都先进金属材料产业技术研究院股份有限公司,四川成都 610300

TB9钛合金 棒线材 微观组织 力学性能 再结晶

2024

材料开发与应用
洛阳船舶材料研究所 中国造船工程学会船舶材料学术委员会

材料开发与应用

CSTPCD
影响因子:0.342
ISSN:1003-1545
年,卷(期):2024.39(4)
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