材料科学技术(英文版)2022,Vol.107Issue(12) :14-25.

In-situ TEM investigation of dislocation loop reaction and irradiation hardening in H2+-He+dual-beam irradiated Mo

Yipeng Li Guang Ran Xinyi Liu Qing Han Xiuyin Huang Yifan Ding
材料科学技术(英文版)2022,Vol.107Issue(12) :14-25.

In-situ TEM investigation of dislocation loop reaction and irradiation hardening in H2+-He+dual-beam irradiated Mo

Yipeng Li 1Guang Ran 1Xinyi Liu 1Qing Han 1Xiuyin Huang 1Yifan Ding1
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作者信息

  • 1. College of Energy,Xiamen University,Xiamen 361102,China;Fujian Research Center for Nuclear Engineering,Xiamen 361102,China
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Abstract

Through in-situ TEM observation during 30 keV H2+-He+dual-beam irradiation at 723 K,the reaction and transformation of dislocation loops in pure Mo were investigated,especially for<100>loops.Ir-radiation could directly cause the formation of 1/2<111>loops and<100>loops,but 1/2<111>loops were dominant.In-situ observation confirmed the formation mechanism of<100>loops,including direct irradiation induced mechanism,1/2<111>loop direct conversion mechanism,and reaction mechanism of two 1/2<111>loops.Meanwhile,the reaction of two 1/2<111>loops to produce<100>loop should not require the strict size similarity condition.The reaction between 1/2<111>loops could also pro-duce 1/2<111>loop,which was essentially a process in which one loop absorbed another one.The yield strength increment caused by irradiation-induced loops was analyzed,and its saturation value reached 0.48 GPa at 0.06 dpa.Compared with single He+irradiation,the number density and average diame-ter of loops increased significantly and more serious damage was caused under the synergistic effect of hydrogen and helium.The mechanism based on in-situ experimental observation was discussed in depth.

Key words

In-situ TEM observation/Dislocation loop/Hydrogen helium irradiation/Molybdenum/Irradiation hardening

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基金项目

Jinchi Huang and Zhe-hui Zhou from the Xiamen University for the support of ion irra-diation experiments and TEM experiments,res()

National Natural Science Foundation of China(11975191)

National Natural Science Foundation of China(U1832112)

National Natural Science Foundation of China(U1967211)

出版年

2022
材料科学技术(英文版)
中国金属学会 中国材料研究学会 中国科学院金属研究所

材料科学技术(英文版)

CSTPCDCSCDSCI
影响因子:0.657
ISSN:1005-0302
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