材料科学技术(英文版)2022,Vol.120Issue(25) :15-35.

Tailoring precipitation/properties and related mechanisms for a high-strength aluminum alloy plate via low-temperature retrogression and re-aging processes

L.G.Hou H.Yu Y.W.Wang L.You Z.B.He C.M.Wu D.G.Eskin L.Katgerman L.Z.Zhuang J.S.Zhang
材料科学技术(英文版)2022,Vol.120Issue(25) :15-35.

Tailoring precipitation/properties and related mechanisms for a high-strength aluminum alloy plate via low-temperature retrogression and re-aging processes

L.G.Hou 1H.Yu 2Y.W.Wang 3L.You 3Z.B.He 3C.M.Wu 4D.G.Eskin 5L.Katgerman 6L.Z.Zhuang 3J.S.Zhang3
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作者信息

  • 1. State Key Laboratory for Advanced Metals&Materials,University of Science&Technology Beijing,Beijing 100083,China;BCAST,Brunel University London,Kingston Lane,Uxbidge Middlesex UB8 3PH,United Kingdom;Nanjing Advanced Transportation Equipment New Technology Research Institute,Nanjing 211800,China
  • 2. Institute of mineral resources,Chinese Academy of Geological Sciences,Beijing 100037,China
  • 3. State Key Laboratory for Advanced Metals&Materials,University of Science&Technology Beijing,Beijing 100083,China
  • 4. Nanjing Advanced Transportation Equipment New Technology Research Institute,Nanjing 211800,China
  • 5. BCAST,Brunel University London,Kingston Lane,Uxbidge Middlesex UB8 3PH,United Kingdom;Tomsk State University,Tomsk,634050,Russian Federation
  • 6. Katgerman Aluminium Technology,van Beuningenlaan 10,2334CC Leiden,NetherlandsDepartment of Materials Science and Engineering,Delft University of Technology,Mekelweg 2,2628CD Delft,the Netherlands
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Abstract

The retrogression and re-aging(RRA)processes,aimed mainly at tailoring intergranular precipitates,could significantly improve the corrosion resistance(i.e.,stress corrosion cracking resistance)without considerably decreasing the strength,which signifies that an efficient control of the size,distribution and evolution of intergranular and intragranular precipitates becomes critical for the integrated prop-erties of the(mid-)thick high-strength Al alloy plates.Compared to RRA process with retrogression at 200℃(T77),this study investigated the impact of a modified RRA process(MT77)with lower ret-rogression temperatures(155-175℃)and first-stage under-aging on the properties of a high-strength AA7050 Al alloy,in combination with detailed precipitate characterization.The study showed that the strength/microhardness of the RRA-treated alloys decreased with raising retrogression temperature and/or prolonging retrogression time,along with the increased electrical conductivity.The rapid responsiveness of microstructure/property typical of retrogression at 200℃was obviously postponed or decreased by using MT77 process with longer retrogression time that was more suitable for treating the(mid-)thick plates.On the other hand,higher retrogression temperature facilitated more intragranular η precipitates,coarse intergranular precipitates and wide precipitate free zones,which prominently increased the elec-trical conductivity alongside a considerable strength loss as compared to the MT77-treated alloys.With the preferred MT77 process,the high strength approaching T6 level as well as good corrosion resistance was achieved.However,though a relatively homogeneous through-thickness strength was obtained,some small discrepancies of properties between the central and surface areas of an 86-mm thick 7050 Al alloy plate were observed,possibly related to the quenching sensitivity.The precipitate evolution and mech-anistic connection to the properties were discussed and reviewed for high-strength Al alloys along with suggestions for further RRA optimization.

Key words

Aluminum alloy/Heat treatment/Precipitation/Strength/Grain boundary

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基金项目

Constructed Project for Key Laboratory of Beijing,China(BJSJ2019004)

State Key Laboratory for Advanced Metals and Materials of China(2018Z-23)

Major State Research and Development Program of China(2016YFB0300801)

国家自然科学基金(51401016)

International Science and Technology Cooperation Projects of Nanjing,China(201818014)

BCAST for hosting L.G()

China Scholarship Council()

出版年

2022
材料科学技术(英文版)
中国金属学会 中国材料研究学会 中国科学院金属研究所

材料科学技术(英文版)

CSTPCDCSCDSCI
影响因子:0.657
ISSN:1005-0302
参考文献量129
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