首页|面向高频应用的Fe-Si-Al软磁粉芯制备工艺改进及性能表征

面向高频应用的Fe-Si-Al软磁粉芯制备工艺改进及性能表征

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为了提升Fe-Si-Al软磁粉芯的抗饱和性能,解决高频下产生较大的磁损耗等问题,本研究利用Al3+水解法制备了氧化铝包覆小粒径Fe-Si-Al粉末制备软磁粉芯工艺,探究了铝源液中氧化铝含量和成型压强对软磁粉芯高频磁性能的影响.运用扫描电子显微镜对经不同氧化铝含量的铝源液水解物包覆处理的Fe-Si-Al粉末表面形貌进行了表征,借助傅里叶红外光谱仪对包覆层成分进行分析.结果表明随着氧化铝含量增加,由包覆层引起的结构退磁场逐渐增大,软磁粉芯的有效磁导率减小,抗磁饱和性能改善;成型压强主要通过影响粉芯内部的气隙率和包覆层的质量来影响粉芯磁性能,压强越大,气隙率越小,有效磁导率越大,但压强过大会破坏粉末表面包覆层,恶化磁性能.经测定氧化铝含量为2.0 wt%、成型压强为1 860 MPa时获得的软磁粉芯的有效磁导率约为60;外加直流磁场强为8 000 A/m时,粉芯的有效磁导率百分比(%μe)高达63.84%;200 kHz/50 mT条件下磁损耗为235.7 mW/cm3.
Process Improvement and Characterization of Fe-Si-Al Soft Magnetic Composites for High Frequency Applications
In order to improve the anti-saturation and solve the problem of high core loss at high frequency of Fe-Si-Al soft magnetic composites,the process of preparing soft magnetic composites by alumina coated small particle size Fe-Si-Al powder was conducted by Al3+hydrolysis method.The effects of alumina content in aluminum sources solution and pressing pressure on the high frequency magnetic properties of soft magnetic composites were studied.The micro-morphology of the powder coated with different amounts of alumina was observed by a scanning electron microscope(SEM),and the chemical composition of the coating was analyzed by a Fourier transform infrared spectrometer(FTIR).The experimental results indicate that with the increase of alumina content,the permeability of soft magnetic composites is reduced,but the DC-bias performance is improved.The reason is that the structural demagnetization caused by the coating increases gradually.The forming pressure mainly affects the magnetic properties by affecting the internal air gap rate and the quality of the coating.The greater the pressure is,the smaller the air gap rate and the greater the magnetic permeability is.However,the surface coating of the powder will be damaged and the magnetic properties will be deteriorated because of excessive pressure.It shows that when the dosage of alumina is 2.0 wt%and the molding pressure is 1 860 MPa,the permeability of the soft magnetic composites is about 60,the%μe of the powder core is up to 63.84%at 8 000 A/m DC magnetic field and the core loss is 235.7 mW/cm3 at 200 kHz/50 mT.

Fe-Si-Al soft magnetic compositesHigh-frequencyInsulation coatingCore lossAnti-seturetion

张学斌、熊汉武、吴鹏、曾旭东、杨富尧、邹中秋、苏海林

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安徽瑞德磁电科技有限公司,安徽 芜湖 241003

国家电网有限公司,北京 100031

国家电网江苏省电力有限公司电力科学研究院,江苏 南京 211103

国家电网智能电网研究院有限公司先进输电技术国家重点实验室,北京 102211

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Fe-Si-Al软磁粉芯 高频 绝缘包覆 磁损耗 抗磁饱和性能

国家电网公司总部科技资助项目

5500-202118252A-0-0-00

2024

材料科学与工程学报
浙江大学

材料科学与工程学报

CSTPCD北大核心
影响因子:0.765
ISSN:1673-2812
年,卷(期):2024.42(3)
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