材料科学与工艺2024,Vol.32Issue(1) :34-41.DOI:10.11951/j.issn.1005-0299.20220386

纳米晶合金粉芯的超重力渗流制备及磁性能

Super-gravity percolation process of nanocrystalline alloy powder cores and magnetic properties

王佳敏 甘章华 朱昭峰 吴传栋 鲁越辉 丁景楠
材料科学与工艺2024,Vol.32Issue(1) :34-41.DOI:10.11951/j.issn.1005-0299.20220386

纳米晶合金粉芯的超重力渗流制备及磁性能

Super-gravity percolation process of nanocrystalline alloy powder cores and magnetic properties

王佳敏 1甘章华 1朱昭峰 2吴传栋 1鲁越辉 1丁景楠1
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作者信息

  • 1. 省部共建耐火材料与冶金国家重点实验室(武汉科技大学),武汉 430081
  • 2. 江苏奥玛德新材料科技有限公司,江苏盐城 224000
  • 折叠

摘要

为了探索粉芯的新制备工艺,以Fe73.5Cu1Nb3Si13.5B9纳米晶合金铁芯为原料,使用机械破碎法制粉,并采用超重力渗流工艺制备了 7种不同粒度配比的纳米晶合金粉芯,借助SEM、XRD、VSM分别对纳米晶粉末的形貌、结构和磁性能进行了表征,研究了粉末粒度配比对纳米晶合金粉芯的形貌、密度、有效磁导率、损耗及品质因数的影响.结果表明,机械破碎法制得的粉末虽带尖角,但矫顽力低,利用超重力渗流工艺制备的粉芯其粉末表面基本被树脂完全包覆.同时,通过适当的粉末粒度匹配,发现性能最佳粉芯的粉末粒度配比为:100~200目占60%,200~400目占20%,400~1 000目占20%.该种粉芯的密度为4.46 g/cm3,在100~3 000 kHz频率范围内有效磁导率比较稳定,且在3 000 kHz时为28.2.当设定磁感应强度为20 mT,频率为500 kHz时,其损耗为99.1 W/kg.另外,根据实验结果可知,该工艺能够制备出频率在MHz以上具有较低损耗的粉芯.

Abstract

To explore a new preparation process of powder cores,Fe73.5Cu1Nb3Si13.5B9 nanocrystalline alloy cores were used as raw material and powdered by mechanical crushing method.Subsequently,seven kinds of nanocrystalline alloy powder cores with different particle size ratios were prepared by super-gravity percolation process.The morphology,structure,and magnetic properties of powder were characterized by SEM,XRD,and VSM,respectively.And the effect of particle size ratio on the morphology,density,effective permeability,core loss and quality factor of powder cores were studied.The results show that the powder prepared by mechanical crushing has low coercivity despite its sharp corners,and the powder surface of powder cores prepared by super-gravity percolation process are essentially solely covered by resin.Moreover,with proper particle size ratio,it is found that the best performance of the powder core's particle size ratio is:100~200 mesh powder accounting for 60%,200~400 mesh powder accounting for 20%,400~1 000 mesh powder accounting for 20%.The density of the core is 4.46 g/cm3 and the effective permeability is relatively stable in the frequency range from 100 kHz to 3 000 kHz,reaching 28.2 at 3 000 kHz.The core loss is only 99.1 W/kg at the magnetic induction strength of 20 mT and the frequency of 500 kHz.Furthermore,this process can produce low-loss powder cores at frequencies above MHz according to the experiment results.

关键词

Fe73.5Cu1Nb3Si13.5B9纳米晶合金/粉芯/超重力渗流/粒度配比/有效磁导率/粉芯损耗

Key words

Fe73.5Cu1Nb3Si13.5B9 nanocrystalline alloy/powder cores/super-gravity percolation process/particle size ratio/effective permeability/core loss

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基金项目

国家自然科学基金资助项目(51904213)

湖北省创新群体项目(2021CFA023)

出版年

2024
材料科学与工艺
中国材料研究学会 哈尔滨工业大学

材料科学与工艺

CSTPCDCSCD北大核心
影响因子:0.491
ISSN:1005-0299
参考文献量7
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