材料研究学报2024,Vol.38Issue(7) :499-507.DOI:10.11901/1005.3093.2023.555

深冷处理对双峰分离非基面织构AZ31镁合金板材室温力学性能的影响

Effect of Cryogenic Treatment on Mechanical Behavior of AZ31 Mg Alloy Sheet with Bimodal Non-basal Texture at Room Temperature

汪丽佳 许君怡 胡励 苗天虎 詹莎
材料研究学报2024,Vol.38Issue(7) :499-507.DOI:10.11901/1005.3093.2023.555

深冷处理对双峰分离非基面织构AZ31镁合金板材室温力学性能的影响

Effect of Cryogenic Treatment on Mechanical Behavior of AZ31 Mg Alloy Sheet with Bimodal Non-basal Texture at Room Temperature

汪丽佳 1许君怡 1胡励 1苗天虎 1詹莎1
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作者信息

  • 1. 重庆理工大学材料科学与工程学院 重庆 400054
  • 折叠

摘要

将经520℃/5 h热处理的双峰分离非基面织构AZ31镁合金板材分别进行水冷处理和在液氮中深冷处理12 h,然后进行室温单轴拉伸实验并使用电子背散射衍射(EBSD)和透射电子显微(TEM)等手段表征,研究其室温力学行为和微观组织的演化.结果表明:在深冷处理和水冷处理的双峰分离非基面织构镁合金板材中,都析出了纳米相(Mg17Al12和Al8Mn5).与水冷处理的板材相比,深冷处理板材中析出相的体积分数提高了65.5%,尺寸增大了 78.7%.6%和12%的室温拉伸结果表明,变形后{10(1)2}拉伸孪晶的体积分数分别提高了38.0%和36.7%.与水冷处理板材相比,深冷处理板材的初始屈服强度和最大抗拉强度分别提高43.8%和5.2%,但是断裂延伸率降低了20.4%.强度提高的主要原因是,在深冷处理过程中生成的高密度位错、Mg17Al12和Al8Mn5纳米析出相产生了沉淀强化;断裂延伸率降低的主要原因是,在{1012}拉伸孪晶界积累的高密度位错阻碍了基面滑移,使微裂纹倾向于向高位错密度处扩展.

Abstract

In the present study,AZ31 Mg-alloy sheets with bimodal non-basal texture were subjected to heating treatment(520℃/5 h),and then immediately water-quenched and quenched into liquid nitro-gen for 12 h.Then,their ambient temperature mechanical performance and microstructure evolution were studied by means of uniaxial tension testing,electron backscatter diffraction(EBSD)and transmis-sion electron microscopy(TEM).The results show that nano-precipitates Mg17Al12 and Al8Mn5 all exist in AZ31 Mg-alloy sheets.However,compared to the Mg-alloy sheet subjected to water-cooling treatment,the volume fraction and size of precipitates increase about 65.5%and 78.7%respectively for the sheet subjected to cryogenic treatment.Meanwhile,the volume fraction of {10(1)2} extension twin(ET)increases by 38.0%and 36.7%for the sheet being subjected to 6%and 12%deformation,respectively.The yield strength(YS)and ultimate tensile strength(UTS)of the cryogenic treated sheets are increased by 43.8%and 5.2%,respectively,compared with the water-cooling treated ones,however,the fracture elongation(FE)decreases by 20.4%.The increase in YS and UTS may mainly be due to the generation of high-den-sity dislocations and precipitation strengthening by Mg17Al12 and Al8Mn5 precipitates during cryogenic treat-ment.The decrease in FE is mainly due to the accumulation of high-density dislocations near {1012} ET boundaries during tensile deformation at room temperature,which would hinder the movement of basal slip and benefit in propagation of microcracks to expand to this region.

关键词

金属材料/非基面织构AZ31镁合金/深冷处理/微观组织演化/塑性变形机制

Key words

metallic materials/non-basal texture AZ31 magnesium alloy/cryogenic treatment/micro-structure evolution/plastic deformation mechanism

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基金项目

重庆市博士后研究项目(2021XM1022)

重庆市教育委员会科学技术研究项目(KJQN202101141)

重庆理工大学科研创新团队培育计划(2023TDZ010)

重庆理工大学校级研究生创新项目(gzlcx20222004)

重庆理工大学大学生创新创业训练计划项目(202311660005)

出版年

2024
材料研究学报
国家自然科学基金委员会 中国材料研究学会

材料研究学报

CSTPCDCSCD北大核心
影响因子:0.605
ISSN:1005-3093
参考文献量4
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