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杜马斯燃烧法测定有机肥料中全氮含量的可行性研究

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考察了杜马斯燃烧法和行业标准《有机肥料》(NY/T 525-2021)中的方法测定有机肥料中全氮含量的精密度和加标回收率.结果表明:NY/T 525-2021 中的方法测得 5 个有机肥料样品的全氮质量分数为1.76%~3.83%,加标回收率为 99.5%~101.0%;杜马斯燃烧法测得 5 个有机肥料样品的全氮质量分数为1.70%~3.84%,加标回收率为 98.1%~104.7%;两种方法的相对标准偏差为 0.18%~2.45%,均可满足有机肥料中全氮含量的测定要求.与NY/T 525-2021 中的方法相比,杜马斯燃烧法具有操作便捷安全、自动化程度高、测定耗时短等特点.
Feasibility Study on Determination of Total Nitrogen Content in Organic Fertilizer by Dumas Combustion Method
The precision and recovery of the determination of total nitrogen content in organic fertilizers by Dumas combustion method and the method in industry standard"Organic Fertilizer"(NY/T 525-2021)are investigated.The results show that the total nitrogen mass fraction of the five organic fertilizer samples measured by the method in NY/T 525-2021 is 1.76%to 3.83%,and the recovery is 99.5%to 101.0%.The mass fraction of total nitrogen in five organic fertilizer samples measured by Dumas combustion method is 1.70%to 3.84%,and the recovery is 98.1%to 104.7%.The relative standard deviation of the two methods is 0.18%to 2.45%,both of which can meet the requirements of the determination of total nitrogen content in organic fertilizer.Compared with the method in NY/T 525-2021,Dumas combustion method has the characteristics of convenient and safe operation,high degree of automation and short measurement time.

organic fertilizerDumas combustion methodtotal nitrogen contentrecovery

杨莹、桂素萍、汪美先、李玉兰

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云南省化工产品质量监督检验站 云南昆明 650228

有机肥料 杜马斯燃烧法 全氮含量 加标回收率

2024

肥料与健康

肥料与健康

ISSN:
年,卷(期):2024.51(3)
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