首页|一步水热法制备MoO3纳米带/还原氧化石墨烯及其电化学性能

一步水热法制备MoO3纳米带/还原氧化石墨烯及其电化学性能

扫码查看
为了提高超级电容器电极材料三氧化钼(MoO3)的储能性能,通过一步水热法合成了 MoO3纳米带/还原氧化石墨烯(reduced graphene oxide,RGO)复合材料,研究了水热法对复合材料的组织结构及电化学性能的影响.利用X射线衍射分析、扫描电子显微形貌观察、傅里叶变换红外光谱分析、循环伏安曲线、恒流充放电曲线等方法对材料的物相、形貌及电化学性能进行了表征.结果显示,通过一步水热法成功制得MoO3纳米带/RGO复合材料,复合前MoO3比电容为228 F·g-1,复合后比电容提高了 17.5%.复合材料中MoO3纳米带被还原氧化石墨烯包裹或者附着在还原氧化石墨烯表面,增强了材料的导电性并使其结构更稳定,从而提升了电化学性能.
Synthesis of MoO3 nanobelts/reduced graphene oxide by one-step hydrothermal method and the corresponding electrochemical properties
To improve the energy storage performance of MoO3 as the supercapacitor electrode materials,the MoO3 nanoribbon/reduced graphene oxide(RGO)composites were synthesized by one-step hydrothermal method.The phase structure,microstructure,and electrochemical properties of the composites were characterized by X-ray diffraction analysis,scanning electron microscopy,Fourier transform infrared spectroscopy,cyclic voltammetry curves,and constant current charge discharge curves.The results show that,the MoO3 nanoribbon/RGO composites are successfully fabricated by the one-step hydrothermal method.Encouragingly,the specific capacitance of the composite materials is increased by 17.5%,compared with that of pure MoO3 as 228 F·g-1.Furthermore,the MoO3 nanoribbons are wrapped by RGO or attached to the surface of RGO in the composites,enhancing the electrical conductivity and structure stability,and then improving the electrochemical performance.

molybdenum trioxidehydrothermal methodgraphene oxidesupercapacitorspecific capacitance

吕星、罗成、梁桂杰

展开 >

湖北文理学院理工学院,襄阳 441053

湖北汽车工业学院材料科学与工程学院,十堰 442002

湖北文理学院低维光电材料与器件湖北省重点实验室,襄阳 441053

三氧化钼 水热合成 氧化石墨烯 超级电容器 比电容

2024

粉末冶金技术
中国机械工程学会,中国金属学会,中国有色金属学会,北京科技大学

粉末冶金技术

CSTPCD北大核心
影响因子:0.341
ISSN:1001-3784
年,卷(期):2024.42(4)
  • 10