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气相色谱HP-5柱快速测定苯乙烯中DNBP含量

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采用色谱柱HP-5分离苯乙烯中DNBP(2-仲丁基-4,6-二硝基苯酚),氢火焰离子检测器(FID)检测、外标法[1]定量,快速测定苯乙烯中DNBP含量.实验结果表明,此方法准确度和精密度较好,分析时间短,满足方法标准[2]要求和工艺控制要求,能成功替代传统分光光度比色法.
Rapid determination of DNBP in styrene by gas chromatography with HP-5 column
DNBP(2-sec-butyl-4,6-dinitrophenol)in styrene was separated by HP-5 column,detected by FID and quantified by external standard method[1],and the content of DNBP in styrene was rapidly determined.The experimental results showed that this method had good accuracy and precision,short analysis time,met the requirements of method standard[2]and process control,and could successfully replace the traditional spectrophotometry.

DNBPHP-5 columnSubstitute

代生平、陈实春、王磊、李建建、杨德浩

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中国石油独山子石化公司质检中心,独山子 833699

DNBP HP-5柱 替代

2023

分析仪器
北京市北分仪器技术有限责任公司(北京分析仪器研究所) 中国仪器仪表行业协会

分析仪器

CSTPCD
影响因子:0.306
ISSN:1001-232X
年,卷(期):2023.(6)
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