首页|微波消解-ICP-OES法测定化妆品中二氧化钛含量

微波消解-ICP-OES法测定化妆品中二氧化钛含量

扫码查看
建立了微波消解-电感耦合等离子体光谱法(ICP-OES)测定化妆品中二氧化钛含量的测试方法.化妆品样品经过混合酸微波消解工艺处理后,采用电感耦合等离子体光谱法(ICP-OES)以测定其中二氧化钛的含量,其线性范围在 0.1 mg/L~2.0 mg/L区间,本方法的相关系数高于0.999,展现出卓越的线性关系;同时其检出限可达至0.94 mg/kg,回收率高达90%~110%,相对标准偏差(RSD)为1.93%~2.32%.结果表明,该方法可批量处理样品,该方法凭借其检测速度高效、灵敏度高以及精密度和准确度优良等优势,能够充分满足化妆品中二氧化钛含量测定的需求.
Microwave Digestion ICP-OES Method for Determining Titanium Dioxide Content in Cosmetics
A novel testing method has been established for determining the content of titanium dioxide in cosmetics through Microwave Digestion-Inductively Coupled Plasma Optical Emission Spectrometry(ICP-OES).The cosmetic samples,after undergoing microwave-assisted digestion with mixed acids,were subjected to ICP-OES analysis to quantify their titanium dioxide content.This method exhibits a linear range spanning from 0.1 to 2.0 mg/L,with an outstanding linearity demonstrated by a correlation coefficient surpassing 0.999.Additionally,it boasts a detection limit as low as 0.94 mg/kg and achieves recovery rates ranging from 90%to 110%,accompanied by relative standard deviations(RSDs)between 1.93%and 2.32%.The results indicate that this method is amenable to batch processing and,due to its attributes of high throughput,sensitivity,precision,and accuracy,it effectively meets the requirements for the determination of titanium dioxide concentrations in cosmetic products.

microwave digestioninductively coupled plasma mass spectrometrytitanium dioxidecosmetics

单瑞娟

展开 >

通标标准技术服务(上海)有限公司,上海 200233

微波消解 电感耦合等离子体发射光谱仪 二氧化钛 化妆品

2024

广东化工
广东省石油化工研究院

广东化工

影响因子:0.288
ISSN:1007-1865
年,卷(期):2024.51(13)