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无机化学综合实验的教改与实践:水滑石的合成与表征

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本论文针对现有的无机化学综合实验《镁铝水滑石的合成》进行了教学改进与实践.改进之处在于以下三点:第一,以共沉淀法代替尿素法制备水滑石,操作简单,能更好地控制溶液的pH值,便于形成稳定的晶型;第二,设计将不同金属阳离子引入层板,以探究二价阳离子对水滑石形貌、晶型和结构的影响,促使学生对知识的理解与整合;第三,拓展使用了 X-射线单晶衍射、傅里叶红外光谱技术和扫描电子显微镜,分析水滑石的晶体结构、官能团和形貌,从而锻炼学生的分析和处理数据的能力.改进后的教学实验缩短了反应时间,现象明显,拓宽了学生科学前沿的视野,有利于培养学生的创新思维能力,提升学生的科学素养,更加符合本科实验教学.
Teaching Reform and Practice of Comprehensive Experiments in Inorganic Chemistry:Synthesis and Characterization of Hydrotalcite
It aims at improving and practice the teaching of the existing inorganic chemistry comprehensive experiment"Synthesis of Magnesium Aluminum Hydrotalcite".The improvement lies in the following three points:firstly,using co precipitation method instead of urea method to prepare hydrotalcite,which is simple to operate and can better control the pH value of the solution,facilitating the formation of stable crystal forms;secondly,design to introduce different metal cations into the laminates to explore the influence of divalent cations on the morphology and structure of hydrotalcite,promoting students'understanding and integration of knowledge;thirdly,the use of X-ray single crystal diffraction,Fourier transform infrared spectroscopy,and scanning electron microscopy was expanded to analyze the crystal structure,functional groups,and morphology of hydrotalcite,thereby enhancing students'ability to analyze and process data.The improved teaching experiment has shortened the reaction time,and the phenomenon is obvious.It has expanded students'horizons at the forefront of science,which is conducive to cultivating their innovative thinking ability,enhancing their scientific literacy,and more in line with undergraduate experimental teaching.

experimental teachinghydrotalciteinorganic chemistry

黄曦明、彭林

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邵阳学院 食品与化学工程学院,湖南 邵阳 422000

实验教学 水滑石 无机化学

2024

广东化工
广东省石油化工研究院

广东化工

影响因子:0.288
ISSN:1007-1865
年,卷(期):2024.51(13)