首页|乳液法制备PDMS/ZIF-8混合基质膜及VOC分离性能综合实验教学设计

乳液法制备PDMS/ZIF-8混合基质膜及VOC分离性能综合实验教学设计

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双碳背景下,挥发性有机物(VOCs)减排受到广泛关注.为此本文设计了乳液法制备 PDMS/ZIF-8 混合基质膜并用于 VOC分离的综合性实验.采用红外光谱、扫描电镜和超景深显微镜对成膜过程、膜结构和形貌进行表征和分析,VOC/N2分离性能测试结果表明PDMA/ZIF-8 膜具有良好的VOC分离性能;随着ZIF-8 添加量的增加,PDMS/ZIF-8 膜的VOC渗透系数呈先减小后增大的趋势,而分离选择性先增大后减小.实验涵盖了文献调研、气体分离膜制备、结构表征分析、性能测试等多种技能训练,可强化学生对化工传质与分离基础知识的理解和拓展,并激发学生的创新潜能,提高学生的自主学习和创新实践等能力.
Experimental Teaching Design for VOC Separation Performance of PDMS/ZIF-8 Mixed Matrix Membranes Prepared by Emulsion Method
Under the background of dual carbon,the emission reduction of volatile organic compounds(VOC)has attracted widespread attention.Therefore,a comprehensive experiment was designed to prepare PDMS/ZIF-8 mixed matrix membrane by emulsion method for VOC separation.The film-forming process,membrane structure and morphology were characterized and analyzed by infrared spectroscopy,scanning electron microscopy and ultra-depth microscopy.The results of the VOC/N2 separation performance test showed that the PDMA/ZIF-8 membrane had good VOC separation performance.With the increase of ZIF-8 content,the VOCs permeability of PDMS/ZIF-8 membrane decreased first and then increased,while the separation selectivity showed the opposite trend.The experiment covers literature research,gas separation membrane preparation,structural characterization analysis,performance testing and other skill training,which can strengthen students'understanding and expansion of basic knowledge of chemical mass transfer and separation,stimulate their innovation potential,and improve their independent learning and innovation practice capabilities.

experimental teaching designmixed matrix membraneVOC separationemulsion membrane formation

白云翔、张春芳

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江南大学,江苏 无锡 214122

实验教学设计 混合基质膜 VOC分离 乳液成膜

2024

广东化工
广东省石油化工研究院

广东化工

影响因子:0.288
ISSN:1007-1865
年,卷(期):2024.51(14)