Detecting Cu,Pbinsurfacewaterby ICP method was experienced,two approaches of preparingstandard curve were carried out with volumetric flask+pipettor method,and colorimetric tube+pipettor gunmethod,The relative uncertainty ofthe former method is urel(Cu)=1.57％,urel(Pb)=2.70％,The relative uncertainty of the later methodis urel(Cu)=1.64％,urel(Pb)=2.09％.The result showed that Cu,Pb had good linear relationship in the concentration range of 0 mg/L～2.0 mg/L.
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