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电感耦合等离子体发射光谱法测定蒙脱石中钛含量

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本研究建立了电感耦合等离子体发射光谱法(ICP-OES)测定蒙脱石中钛(Ti)元素含量的检测方法.实验结果表明该方法线性关系良好,相关系数(r)大于0.999;钛元素的检出限和定量限分别为0.0965 和0.318 mg·kg-1;精密度和重复性的相对标准偏差(RSD)分别为0.676%和2.29%,加标回收率为99.69%.以上结果说明该方法检出限低,精密度和准确度高,是检测蒙脱石以及类似矿物样品钛元素的理想分析方法.
Determination of Titanium Content in Montmorillonite by Inductively Coupled Plasma Optical Emission Spectrometry
A detection method for determining titanium in montmorillonite by inductively coupled plasma optical emission spectroscopy(ICP-OES)has been established.The experimental results show that the method has a good linear relationship,and the correlation coefficient(r)is greater than 0.999;The detection limit and quantification limit of titanium element are 0.0965 and 0.318 mg·kg-1,respectively;The relative standard deviation(RSD)of precision and repeatability were 0.676%and 2.29%,respectively,and the recovery rate of samples was 99.69%.The above results indicate that this method has a low detection limit,high precision and accuracy,and is an ideal analytical method for detecting titanium elements in montmorillonite and similar mineral samples.

montmorilloniteinductively coupled plasma optical emission spectroscopytitanium

马继承、马婧、王爱霞

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东北师范大学化学学院,吉林 长春 130024

吉林省实验中学,吉林 长春 130024

蒙脱石 电感耦合等离子体发射光谱

2024

广东化工
广东省石油化工研究院

广东化工

影响因子:0.288
ISSN:1007-1865
年,卷(期):2024.51(18)