广东化工2024,Vol.51Issue(19) :178-179,191.DOI:10.3969/j.issn.1007-1865.2024.019.057

吴茱萸挥发油的GC-MS分析

GC-MS Analysis of the Volatile Oil of Euodiae Fructus

尹丽 彭苑霞 陆华强 杨秋燕 曹亮启
广东化工2024,Vol.51Issue(19) :178-179,191.DOI:10.3969/j.issn.1007-1865.2024.019.057

吴茱萸挥发油的GC-MS分析

GC-MS Analysis of the Volatile Oil of Euodiae Fructus

尹丽 1彭苑霞 1陆华强 2杨秋燕 1曹亮启1
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作者信息

  • 1. 广州华商职业学院,广东 广州 511300
  • 2. 广州中医药大学岭南中药资源教育部重点实验室,广东 广州 510700
  • 折叠

摘要

为分析不同干燥方法处理的吴茱萸挥发油成分,采用水蒸气蒸馏法提取烘干、晒干处理的吴茱萸的挥发油,利用气相色谱-质谱联用技术(GC-MS)检测两者挥发油成分,采用面积归一化法计算各成分的相对含量;结果表明两者挥发油的提取率分别为0.21%和 0.29%;从两者挥发油中鉴定到的交集化合物有 65种,但含量差异较大;两者中相对含量前三的化合物相同,分别是β-榄香烯、β-石竹烯和大根香叶烯D;其中含量最高的β-榄香烯具有良好的抗肿瘤作用.本研究为吴茱萸挥发油的开发利用提供了实验基础.

Abstract

In order to analyze the volatile oil components of Euodiae Fructus treated by different drying methods,the volatile oil of oven-drying and sun-drying samples was extracted by water steam distillation,detected by GC-MS method and the relative content of each component was calculated by area normalization method;The results show that the extraction rate of the volatile oils was 0.21%and 0.29%,respectively;65 overlapping compounds were identified from both volatile oil,but the content differences were significant.The top three compounds with the highest relative content in both samples were the same,including β-Elemene,Caryophyllene and Germacrene D;The highest content,β-Elemene,shows good anti-tumor effect.This study provides the experiental basis for the development and utilization of volatile oil from Euodiae Fructus.

关键词

吴茱萸/挥发油/GC-MS/β-榄香烯/β-石竹烯/大根香叶烯D

Key words

Euodiae Fructus/volatile oil/GC-MS/β-Elemene/Caryophyllene/Germacrene D

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基金项目

广东省中药材产业化基地建设项目(粤工信消费函[2021]72号)

2022年度科教研繁荣计划(KY2022018)

出版年

2024
广东化工
广东省石油化工研究院

广东化工

影响因子:0.288
ISSN:1007-1865
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