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液相色谱法测定纺织品中甾醇含量

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通过确定植物甾醇3种主要成分(β-谷甾醇、菜油甾醇、豆甾醇)标准品的液相色谱分析条件,以特征保留时间确定各类甾醇相应的液相色谱指纹图谱.建立了纺织品中甾醇含量的测定方法:以相同液相色谱分析条件对纺织样品提取液进样分析,以各类甾醇标准品指纹图谱为基础,并以外标法求得纺织品中不同类别甾醇含量,最终获得纺织品中甾醇总的含量(质量分数).测定方法精密度和回收率均满足相关标准要求,可用于纺织品中甾醇含量的检测.
Determination of Sterol content in textiles by HPLC
The HPLC analysis conditions of three types of main components of phytosterols(β-sitosterol,canola sterol,stigasterol)were determined,and the corresponding HPLC fingerprints of each type of sterols were determined according to the characteristic retention time.A method for the determination of sterols in textiles was established.The different sterols in textiles were quantified based on the fingerprint of various sterols and external standard method,and the total sterols were obtained.The precision and recovery rate of the method met the requirements of the relevant standards and could be used for the determination of sterol content in textiles.

HPLCtextilessterolcontent(mass fraction)determination

贺志鹏、刘蒙

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中国纺织信息中心(中国)

中联品检(北京)检验技术有限公司(中国)

液相色谱法 纺织品 甾醇 含量(质量分数)测定

2024

国际纺织导报
东华大学

国际纺织导报

影响因子:0.095
ISSN:1007-6867
年,卷(期):2024.52(2)
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