夏天无滴丸的提取工艺研究
The Study on Extraction Process of Decumbent Corydalis Rhizome Dropping Pills
胡佳 1何涛 1于世海2
作者信息
- 1. 辽宁省锦州市食品药品检验所 锦州 121000
- 2. 辽宁康辰药业有限公司 丹东 118301
- 折叠
摘要
目的：研究并建立夏天无滴丸的最佳提取工艺。方法紫外分光光度法测定夏天无总生物碱的含量；高效液相色谱法同时测定夏天无原阿片碱和延胡索乙素的含量。结果最佳提取条件为A3 B1 C3 D2，即浸泡时间为48小时，药材粒度约为20目，渗漉溶液的体积为12倍量药材，渗漉的速度为1．5ml／min。结论为夏天无滴丸的最佳提取工艺的确立提供依据。
Abstract
Objective To study the best extraction process of decumbent corydalis rhizome dropping pills .Methods UV was used to measure total alkaloid content of decumbent corydalis rhizome .HPLC was used to measure the content of corydalis and tetrahydropalmatine . Results The best extract condition is A3B1C3D2, soak time is 48 hours, granularity is 20 item, percolation solution volume is 12 times the amount of medicine , and percolation speed is 1.5ml/min.Conclusion It provided the basis for the establishment of the best extraction process for the decumbent corydalis rhizome dropping pills .
关键词
夏天无/滴丸/高效液相/提取工艺Key words
Decumbent corydalis rhizome/Dropping pills/HPLC/Extraction process引用本文复制引用
出版年
2016
国家科技期刊平台
NSTL
维普
万方数据