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氟化镧铈抛光粉的焙烧制备及抛光性能研究

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采用X射线粉末衍射(XRD)、扫描电子显微镜(SEM)、原子发射光谱仪(AES)等测试技术对氟化镧铈抛光粉产物进行理化性能表征,通过无机晶体结构数据库计算产物的空间结构,用接触角测量仪、表面缺陷检测仪测定了抛光粉体的润湿性能及抛光性能.结果表明,产物均为类球状——400,500,600,700,750 ℃焙烧温度下得到二氧化铈(CeO2)和氟化镧(LaF3)的混合产物(CeO2+LaF3);800,850,900,950,1 000,1 050 ℃焙烧温度下,产物为二氧化铈(CeO2)和氟氧化镧(LaOF)的混合抛光产物(CeO2+LaOF),通过计算获得不同晶型的抛光产物的XRD图及其空间结构.用接触角测量仪获得500,850,1 000 ℃焙烧温度下的产物的润湿性能,用表面缺陷检测仪对500,850,1 000 ℃焙烧温度下的产物对玻璃表面进行抛光,发现温度为850 ℃的抛光效果最好.
Preparation and polishing performance of lanthanum cerium fluoride polishing powder
Properties of physical and chemical for lanthanum cerium fluoride polishing powder were characterized by techniques of X-ray diffraction,scanning electron microscopy.Space structures were calculated by the inor-ganic crystal structure database(ICSD),and wettability and polishing performance was done using contact an-gle measuring equipment and surface defect detector.It was found that the materials are all made up of agglom-erated near-spherical particles.Below 800 ℃,the product is a mixture of cubic CeO2 and trigonal LaF3,while a-bove 800 ℃,it is a mixture of cubic CeO2 and tetragonal LaOF.When the calcination temperature is 850 ℃,the polishing properties of the products is the best.

calcination preparationX-ray diffractionperformancestructure

梅燕、陈文娟、陈学安

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北京工业大学材料科学与工程学院,北京 100124

制备 X射线粉末衍射 性能 结构

国家重点研发计划项目

2021YFB3501102

2024

功能材料
重庆材料研究院 中国仪器仪表学会仪表材料学会

功能材料

CSTPCD北大核心
影响因子:0.918
ISSN:1001-9731
年,卷(期):2024.55(1)