功能材料2024,Vol.55Issue(4) :167-173.DOI:10.3969/j.issn.1001-9731.2024.04.020

纯水相Ag+/TiO2溶液的制备及其抗菌性能研究

Preparation and antibacterial properties of pure aqueous Ag+/TiO2 solution

吴世斌 谢镇泽 王景光 杜昶
功能材料2024,Vol.55Issue(4) :167-173.DOI:10.3969/j.issn.1001-9731.2024.04.020

纯水相Ag+/TiO2溶液的制备及其抗菌性能研究

Preparation and antibacterial properties of pure aqueous Ag+/TiO2 solution

吴世斌 1谢镇泽 1王景光 1杜昶1
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作者信息

  • 1. 华南理工大学材料科学与工程学院,广州 510006
  • 折叠

摘要

采用低温液相法制备了纯水相纳米TiO2溶液,然后在纳米TiO2表面沉积Ag+获得了纯水相Ag+/TiO2溶液.通过扫描电子显微镜(SEM)、X射线能谱仪(EDS)、X射线衍射仪(XRD)、X射线光电子能谱仪(XPS)、傅里叶变换红外光谱仪(FT-IR)、紫外-可见光吸收光谱仪(UV-Vis)和荧光光谱仪(PL)进行表征.经过各项表征分析可知,Ag+/TiO2粒子是粒径10 nm的球形颗粒,XRD特征峰为锐钛矿二氧化钛和硫酸银的叠加峰.此外,沉积的Ag以+1的价态存在,且提高了纳米TiO2的光催化活性,产生了协同效应.抗菌测试结果表明,制备的纯水相Ag+/TiO2溶液在不同菌种和不同应用环境下均表现优异的抗菌性能,说明了 Ag+/TiO2抗菌的高效性和广谱性,具有极大的市场应用价值.

Abstract

Pure aqueous nano-TiO2 solution was prepared by low temperature liquid phase method,and then Ag+was deposited on nano-TiO2 surface to obtain pure aqueous Ag+/TiO2 solution.It was characterized by scanning electron microscopy(SEM),X-ray energy spectrometer(EDS),X-ray diffractometer(XRD),X-ray photoelectron spectrometer(XPS),Fourier transform infrared spectrometer(FT-IR),Ultraviolet-visible light absorption spectrometer(UV-Vis)and fluorescence spectrometer(PL).After various characterization analysis,it can be seen that Ag+/TiO2 particles are spherical particles with a particle size of 10 nm,and the XRD charac-teristic peak is the superposition peak of anatase titanium dioxide and silver sulfate.In addition,the deposited Ag exists in the valence state of+1,and the photocatalytic activity of nano-TiO2 is improved,resulting in a synergistic effect.The results of antibacterial test show that the prepared pure aqueous Ag+/TiO2 solution has excellent antibacterial performance in different strains and different application environments,indication the high efficiency and broad spectrum of Ag+/TiO2 antibacterial,which has great market application value.

关键词

Ag+/TiO2溶液/低温液相/表面沉积/纯水相/抗菌

Key words

Ag+/TiO2 solution/low temperature liquid phase/surface deposit/pure aqueous phase/antibiosis

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基金项目

国家重点研发计划(2017YFC1105000)

出版年

2024
功能材料
重庆材料研究院 中国仪器仪表学会仪表材料学会

功能材料

CSTPCD北大核心
影响因子:0.918
ISSN:1001-9731
参考文献量1
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