功能材料2024,Vol.55Issue(7) :7001-7007.DOI:10.3969/j.issn.1001-9731.2024.07.001

稀释剂用量对铁硅铝软磁粉芯含浸强度的影响

Effect of diluent dosage on strength of Fe-Si-Al soft magnetic powder core

李梦冉 李睿卿 张学斌 刘伟 张华 邹中秋 苏海林
功能材料2024,Vol.55Issue(7) :7001-7007.DOI:10.3969/j.issn.1001-9731.2024.07.001

稀释剂用量对铁硅铝软磁粉芯含浸强度的影响

Effect of diluent dosage on strength of Fe-Si-Al soft magnetic powder core

李梦冉 1李睿卿 1张学斌 2刘伟 1张华 3邹中秋 3苏海林2
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作者信息

  • 1. 合肥工业大学材料科学与工程学院,合肥 230009
  • 2. 合肥工业大学材料科学与工程学院,合肥 230009;江苏瑞德磁性材料有限公司淮安市软磁粉芯与器件工程技术研究中心,江苏盱眙 211700
  • 3. 江苏瑞德磁性材料有限公司淮安市软磁粉芯与器件工程技术研究中心,江苏盱眙 211700
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摘要

金属软磁粉芯生坯强度通常较低,在制造过程中需采用含浸树脂的方法提高强度.采用非活性稀释剂(四氯乙烯)和活性稀释剂636(三羟甲基丙烷三缩水甘油醚)作为135环氧树脂/甲基四氢苯酐含浸体系的混合稀释剂,研究了四氯乙烯的用量对于铁硅铝软磁粉芯抗压强度的影响以及含浸工艺对铁硅铝软磁粉芯磁性能的影响.同时,结合实测抗压强度和孔隙率对复合材料抗压强度公式进行了修正,得出了金属软磁粉芯抗压强度的计算公式.结果表明,经含浸处理后,软磁粉芯的抗压强度显著提高,在树脂与稀释剂的质量比约为1∶2时达到最大值18.43 MPa,且磁性能与含浸之前的样品相比没有明显变化.这表明在该配比下,稀释剂可以和环氧树脂充分均匀混合,并且可以与固化剂更好地发生交联固化,从而有效提高环氧树脂的力学性能.对含浸工艺和软磁粉芯抗压强度计算公式的研究结果,可为提高软磁粉芯强度的量产工艺开发提供参考.

Abstract

Soft magnetic powder core generally has a low strength,which is improved by using the resin impreg-nation process.In this study,inactive diluent(tetrachloroethylene)and active diluent 636(trimethylol propane triglycidyl ether)were used as the mixed diluent of the 135 epoxy resin/methyltetrahydrophthalic anhydride im-pregnated system,and the influence of the dosage of tetrachloroethylene on the compressive strength and the influence of impregnation process on the magnetic properties for Fe-Si-Al powder cores were studied.In addi-tion,the formula for calculating the actual compressive strength of soft magnetic powder core was modified based on the measured compressive strength and porosity.The results show that the compressive strength of the powder core is greatly improved by the impregnation process,while the magnetic properties change slightly.When the mass ratio of resin to diluent is about 1∶2,the core compressive strength reaches a maximum value of 18.43 MPa.This indicates that the diluent can be fully and evenly mixed with the epoxy resin,and can be cross-linked and cured better with the curing agent at this ratio,which improves the mechanical properties of the epoxy resin accordingly.The research results on impregnation process and formula for calculating the com-pressive strength of soft magnetic powder cores in this paper can provide reference for the development of mass production processes to improve the strength of soft magnetic powder cores.

关键词

金属软磁粉芯/含浸/抗压强度/四氯乙烯

Key words

metallic soft magnetic powder core/liquid impregnation method/compressive strength/tetrachloroeth-ylene

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基金项目

淮安市2021年重点研发计划(工业类)项目(HAG202114)

出版年

2024
功能材料
重庆材料研究院 中国仪器仪表学会仪表材料学会

功能材料

CSTPCD北大核心
影响因子:0.918
ISSN:1001-9731
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