首页|基于GC-FID的便携式总烃、甲烷和非甲烷总烃检测仪校准方法探讨

基于GC-FID的便携式总烃、甲烷和非甲烷总烃检测仪校准方法探讨

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挥发性有机物是当前阶段环境污染治理、监管监测的主要目标物之一,其对环境危害主要是通过形成光化学烟雾,破坏臭氧层、增强温室效应、并可引发雾霾天气.挥发性有机物种类繁多,目前主要以总烃、甲烷和非甲烷总烃的形式进行监测.在现场监测中,使用较多的是采用气相色谱-氢火焰离子化检测器(GC-FID)的便携式总烃、甲烷和非甲烷总烃检测仪,具有检测范围广、分析周期短的优点.使用中需要经常对其进行校准.根据分析原理,目前使用的校准方法主要有两种:即单点校准法和多点曲线校准法.文章以实际校准实验为例,通过对比两种不同校准方法对测量结果的影响,为应用中研究更合适校准方法提供参考.
Discussion on calibration method of portable total hydrocarbon、methane and non-methane total hydrocarbon detector based on GC-FID
Volatile organic compounds are one of the main targets of environmental pollution control,su-pervision and monitoring at the current stage.It can destroy the ozone layer,enhance the greenhouse effect,and lead to haze weather.There are many types of Volatile organic compounds.At present,it is mainly monitored in the form of total hydrocarbon,methane and non-methane total hydrocarbon.During on-site monitoring,the portable total hydrocarbon,methane and non-methane total hydrocarbon detec-tors using gas chromatography-hydrogen flame ionization detector(GC-FID)are widely used,because it has the advantages of wide detection range and short analysis period.It needs to be calibrated frequently in use.According to the analysis principle,there are two main calibration methods used at present:sin-gle-point calibration method and multi-point curve calibration method.In this paper,a practical calibra-tion experiment is taken as an example to compare the effect of two different calibration methods on the measurement results.

GC-FIDportable total hydrocarbonmethane and non-methane total hydrocarbon detectorcalibration method

班继民、陈雨、张朝瑞

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河南省计量测试科学研究院,河南郑州 450000

GC-FID 便携式总烃 甲烷和非甲烷总烃检测仪 校准方法

2024

工业计量
冶金自动化研究设计院 中国计量协会

工业计量

影响因子:0.256
ISSN:1002-1183
年,卷(期):2024.34(4)