首页|红姜花中黄酮的分离与鉴定

红姜花中黄酮的分离与鉴定

扫码查看
风干粉碎后的红姜花(Hedychium coccineum)根茎用工业甲醇浸提,甲醇浸提物用乙酸乙酯-水萃取.采用多种分离技术(硅胶柱层析、Sephadex LH-20、RP-18柱层析、HPLC)分离乙酸乙酯浸膏中的化学成分,通过NMR等方法对所得的化合物进行结构鉴定.共鉴定6个黄酮类化合物,分别是 5-hydroxy-3,7,4'-trimethoxyflavone(1)、3,5-dihydroxy-7,4'-dimethoxyflavone(2)、kaempferol-4'-O-methylether(3)、ermanin(4)、dihydrokaempferide(5)、aromadendrin-7,4'-dimethyl ether(6).均为首次从红姜花中分离得到.
Isolation and Identification of Flavonoids from Hedychium coccineum
The air-dried and crushed rhizomes of Hedychium coccineum were extracted with MeOH,and the extract was partitioned with EtOAc-H2O.The EtOAc extract was isolated by various separation techniques(Silica gel,Sephadex LH-20,RP-18 column chromatography and HPLC).By means of spectroscopic analysis,the isolated compounds were identi-fied as 5-hydroxy-3,7,4'-trimethoxyflavone(1),3,5-dihydroxy-7,4'-dimethoxyflavone(2),kaempferol-4'-O-methylether(3),ermanin(4),dihydrokaempferide(5)and aromadendrin-7,4'-dimethyl ether(6).All the compounds were isolated from H.coccineum for the first time.

Hedychium coccineumchemical constituentflavonoid

郑丽、周日海、张婉婷、张金凤、彭伟、陈业高

展开 >

云南师范大学 化学化工学院,云南 昆明 650500

红姜花 化学成分 黄酮

云南省高等学校药用活性分子结构多样性研究重点实验室项目云南师范大学大学生科研训练基金

KX2022022

2024

海南师范大学学报(自然科学版)
海南师范大学

海南师范大学学报(自然科学版)

影响因子:0.271
ISSN:1674-4942
年,卷(期):2024.37(1)
  • 22