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高强无磁不锈钢Cr21Ni13Mn5Mo2N的热加工特性

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利用Gleeble 3800热模拟机对奥氏体不锈钢Cr21Ni13Mn5Mo2N进行热压缩实验,研究该钢种的高温变形与应变速率以及温度的关系,建立了双曲正弦本构方程,最终得到其热激活能为679.58 kJ/mol,应变速率因子 Z=(ε)exp(679 580/RT).实验结果表明,在 950~1 200 ℃,0.01~10 s-1条件内,材料变形过程均发生动态再结晶,在950 ℃,应变速率为0.1 s-1条件下,再结晶开始的变形量为10%.流变应力随温度升高及应变速率降低呈现明显下降趋势,由950 ℃、10 s-1时的326 MPa降低至1 200℃、0.01 s-1时的75 MPa.结合微观组织分析及锻造试验,对压缩试样开裂问题进行深入探究,结果表明晶界处碳、氧化物的聚集恶化晶界塑性,导致热变形过程中在该处形成裂纹源并逐步扩展.通过热处理和热变形试验,确定Cr21Ni13Mn5Mo2N电渣锭在1 170 ℃固溶6 h后晶界碳、氧化物消除,电渣锭晶界处结合力明显提升,成功消除锻造开裂问题,实现锻造成材率大幅提升.
HOT WORKING CHARACTERISTICS OF HIGH-STRENGTH NON-MAGNETIC STAINLESS STEEL Cr21Ni13Mn5Mo2N
The Gleeble 3800 thermal simulator was used to conduct hot compression experiments on austenitic stainless steel Cr21Ni13Mn5Mo2N.The relationship between high-temperature deformation,strain rate,and temperature of the steel was studied,and a hyperbolic sine constitutive equation was established.Finally,the thermal activation energy was 679.58 kJ/mol,and the strain rate factor Z parameter was=(ε)exp(679 580/RT).The experimental results show that dynamic recrystallization occurs during the deformation process of the material at 950~1 200 ℃ and 0.01~10 s-1 conditions.At 950 ℃ and a strain rate of 0.1 s-1,the deformation amount at the beginning of recrystallization is 10%.The rheological stress shows a significant downward trend with increasing temperature and decreasing strain rate,decreasing from 326 MPa at 950 ℃and 10 s-1 to 75 MPa at 1200 ℃ and 0.01 s-1.By combining microstructure analysis and forging experiments,the cracking problem of compressed specimens was thoroughly investigated.The results showed that the aggregation of carbon and oxides at grain boundaries worsened the plasticity of grain boundaries,leading to the formation of crack sources and gradual expansion at this location during hot deformation.Through heat treatment and hot deformation tests,it was determined that the carbon and oxide at the grain boundaries of Cr21Ni13Mn5Mo2N electroslag ingots were eliminated after 6 hours of solid solution at 1 170 ℃.The bonding force at the grain boundaries of the electroslag ingots was significantly improved,and the problem of forging cracking was successfully eliminated,achieving a significant increase in the yield of forging.

stainless steelCr21Ni13Mn5Mo2Ncompression thermal simulationconstitutive equationhot working plasticity

嵇爽、韩彦光、陈文、赵英利、马瑞楠、周文慧

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河钢材料技术研究院,河北石家庄 050023

河钢宣钢特种材料研究制造公司,河北张家口 075199

不锈钢Cr21Ni13Mn5Mo2N 压缩热模拟 本构方程 热加工塑性

2024

河北冶金
河北省冶金学会

河北冶金

影响因子:0.124
ISSN:1006-5008
年,卷(期):2024.(5)