合成树脂及塑料2024,Vol.41Issue(2) :30-33.DOI:10.19825/j.issn.1002-1396.2024.02.07

基于AFM-IR的高分子聚合物添加剂定量检测新方法

A new method for quantitative detection of polymer additives based on AFM-IR

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合成树脂及塑料2024,Vol.41Issue(2) :30-33.DOI:10.19825/j.issn.1002-1396.2024.02.07

基于AFM-IR的高分子聚合物添加剂定量检测新方法

A new method for quantitative detection of polymer additives based on AFM-IR

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作者信息

  • 1. 中石化(北京)化工研究院有限公司,北京 100013
  • 折叠

摘要

基于原子力-红外检测平台开发了一种定量检测聚合物中少量添加剂的方法.通过表征不同抗氧剂168含量的聚丙烯试样,统计不同试样特征红外吸收峰处的红外图像高亮点占比和平均信号强度变化,成功绘制了抗氧剂含量标准曲线,拟合度高达0.996 7,这一方法可用于未知试样中不同添加剂含量的检测.

Abstract

A quantitative detection method for trace additives in polymers was established based on the atomic force microscopy-infrared spectroscopy(AFM-IR)detection platform.The proportion of high-light points and the average signal intensity at different infrared absorption wavelengths were statistically analyzed by characterizing polypropylene samples with different concentrations of antioxidant 168.The standard curve of antioxidant concentration was successfully drawn with a high fitting degree of 0.996 7.This method can be used for detecting different additives in unknown samples.

关键词

原子力-红外技术/抗氧剂/聚丙烯/定量检测

Key words

atomic force microscopy-based infrared spectroscopy/antioxidant/polypropylene/quantitative detection

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出版年

2024
合成树脂及塑料
中国石化集团资产经营管理有限公司北京燕山石化分公司 橡塑新型材料合成国家工程研究中心

合成树脂及塑料

CSTPCD北大核心
影响因子:0.384
ISSN:1002-1396
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参考文献量21
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