核电子学与探测技术2024,Vol.44Issue(6) :1107-1111.

2022年IAEA国际比对γ谱分析结果及思考

Reflection on the Gamma-ray Spectrometry Analysis Results of the IAEA Annual Proficiency Test and Comparison Exercises

史晓东 陈群 杨小勇 马加一
核电子学与探测技术2024,Vol.44Issue(6) :1107-1111.

2022年IAEA国际比对γ谱分析结果及思考

Reflection on the Gamma-ray Spectrometry Analysis Results of the IAEA Annual Proficiency Test and Comparison Exercises

史晓东 1陈群 1杨小勇 1马加一1
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作者信息

  • 1. 江苏省疾病预防控制中心,南京 210009
  • 折叠

摘要

对 2022 年国际原子能机构(IAEA)国际比对测试中的γ谱分析进行总结,为以后的检测和比对组织工作提供参考.使用高纯锗 γ 谱仪,采用相对比较法,对 3 种不同水样中的 60 Co、134 Cs、137 Cs、210 Pb、241 Am的活度浓度进行了检测.各核素检测结果与目标值的相对偏差范围为-15.25%~8.95%,可接受率 100%,对于传统上采用放化方法测量的210 Pb,本次使用γ谱测量,与目标值的相对偏差为 8.95%.对于质控样中给出的核素,采用相对比较法得到的结果相对偏差较小,由比对组织者提供统一的质控样可有效减小比对结果中由标准品溯源带来的误差.

Abstract

The objective is to summarize the gamma-ray spectrometry analysis results in the 2022 IAEA comparison exercises and provide a reference for future testing and comparison exercises organization work.Methods activity concentration of five radionuclides,60 Co,134 Cs,137 Cs,210 Pb,and 241 Am,in 3 different samples were measured by HPGe γ spectrometry and analyzed with relative comparison methods under the condition of the mixture quality control source.Results are the relative deviations(Bias)between the reported and the target value were within -15.25%~8.95%,which were 100%accepted.210 Pb,which has traditionally been measured using radiochemical methods,was measured by HPGe γ spectrometry this time with a Bias of 8.95%.Conclusions have achieved that for the radionuclides spiked in the quality control sample,the relative deviations between the values analyzed with relative comparison methods and the target values were relatively small.Therefor,using the uniform quality control samples provided by the comparison organizers can effectively reduce the deviation caused by the traceability of the standard samples in the results.

关键词

放射性核素/γ谱分析/国际比对

Key words

radionuclides/gamma-ray spectrum analysis/international comparison exercises

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出版年

2024
核电子学与探测技术
中核(北京)核仪器厂

核电子学与探测技术

北大核心
影响因子:0.215
ISSN:0258-0934
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