首页|量热弹-电位滴定法测定可生物降解胶带中氟含量研究

量热弹-电位滴定法测定可生物降解胶带中氟含量研究

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建立了一种基于量热弹-电位滴定仪检测可降解生物胶带中氟元素的方法.通过一系列实验设计,建立了标准曲线,确定了该方法的检出限和定量限、精密度、准确度,并进行了回收率评估.最终确认了检测方法,试样前处理方法和仪器分析条件,并进行了实际试样的检测.实验结果符合GB/T 27417-2017《合格评定 化学分析方法确认和验证指南》要求.该方法操作简单,可靠性高,可弥补当前标准检测方法的空白.
Study on Determination of Fluorine Content in Biodegradable Tape by Calorimetric Bomb-Potentiometric Titration Method
In this study,a method based on calorimetry bomb-potentiometric titration was established to detect fluorine in biodegradable tape.Through a series of experimental designs,a standard curve was established,and the detection and quantification limits,precision,and accuracy of the method were determined.The recovery rate was also evaluated.Finally,the testing method,sample pre-treatment method,and instrument analysis conditions were confirmed,and actual sample testing was conducted.The experimental results comply with the requirements of GB/T 27417-2017"Guidelines for Confirmation and Validation of Chemical Analysis Methods for Conformity Assessment"This method is simple to operate,highly reliable,and can fill the gap in current standard detection methods.

biodegradable tapefluorinecalorimetric bombpotentiometric titration

蔡佳梓、梁其湛、王沛雯、陈妙兰、陈超青

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广东省江门市质量计量监督检测所,广东江门 529000

广东江门中医药职业学院,广东江门 529000

五邑大学生物科技与大健康学院,广东江门 529020

江门市食品检验所,广东江门 529000

广东省应对技术贸易壁垒协会,广东广州 510655

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可生物降解胶带 氟元素 量热弹 电位滴定

广东省市场监督管理局科研攻关项目五邑大学大学生创新创业训练计划

2023ZZ10202211349206

2024

化工设计通讯
湖南化工医药设计院

化工设计通讯

影响因子:0.126
ISSN:1003-6490
年,卷(期):2024.50(3)
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