化工新型材料2025,Vol.53Issue(1) :100-104.DOI:10.19817/j.cnki.issn1006-3536.2025.01.040

聚酰亚胺固化成型密封用有机硅密封剂的研制

Development and preparation of the silicone sealant for polyimide curing and molding seals

王磊 任河 孙全吉 范召东
化工新型材料2025,Vol.53Issue(1) :100-104.DOI:10.19817/j.cnki.issn1006-3536.2025.01.040

聚酰亚胺固化成型密封用有机硅密封剂的研制

Development and preparation of the silicone sealant for polyimide curing and molding seals

王磊 1任河 1孙全吉 1范召东1
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作者信息

  • 1. 北京航空材料研究院股份有限公司,北京 100095
  • 折叠

摘要

通过耐高温抗氧化、抗密闭降解体系和催化剂体系研究,制备得到一种聚酰亚胺固化成型用有机硅密封剂,并对其密封性能进行了考核验证.研制得到的有机硅密封剂耐温等级可达380℃,在350℃ ×24h老化后仍具备一定弹性,具备优异的耐高温抗密闭降解性能.此外,该有机硅密封剂在高达380℃的聚酰亚胺固化温度下,3MPa的压力下,能够保证热压罐成型工艺所需的密封作用,满足聚酰亚胺复合材料的批量固化成型的需求.

Abstract

Through the study on the high-temperature resistant system,anti-sealing degradation system and catalyst system,a silicon sealant for polyimide curing and molding was prepared,and the sealing property of the silicone sealant was evaluated and verified.The prepared silicone sealant exhibited a temperature resistance of up to 380℃,and still retained a certain extent of elasticity after aging at 350℃ for 24h,demonstrating excellent high-temperature resistance and anti-sealing degradation properties.Moreover,the silicone sealant could ensure the sealing effect required by hot-press can molding process at a polyimide curing temperature of up to 380℃ and a pressure of 3MPa,which met the demands of the batch preparation of polyimide composites.

关键词

耐高温/抗密闭降解/有机硅密封剂/聚酰亚胺/密封

Key words

high-temperature resistant/anti-sealing degradation/silicone sealant/polyimide/sealing

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出版年

2025
化工新型材料
中国化工信息中心

化工新型材料

CSCD北大核心
影响因子:0.357
ISSN:1006-3536
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