A method was developed for determining 25 kinds of sulfonamides and quinolones in environmen-tal water by solid phase extraction-ultra performance liquid chromatography-tandem mass spectrometry.By opti-mizing the experiment conditions,the method had good linearity in the range of 2.00 µg/L～200 pg/L.The method detection limits ranged from 1.01 ng/L to 2.85 ng/L,and the RSDs of 7 measurements ranged from 2.3％to 8.0％.The method was applied in determining tap water and surface water,and the results were not detected.The spiked recoveries with high and low mass concentration levels were 61.2％～102％.
关键词
磺胺类抗生素/喹诺酮类抗生素/固相萃取/超高效液相色谱串联质谱法/水质
Key words
Sulfonamides/Quinolones/Solid phase extraction/Ultra performance liquid chromatography-tandem mass spectrometry/Water quality
维普
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