航空制造技术2024,Vol.67Issue(14) :51-58.DOI:10.16080/j.issn1671-833x.2024.14.051

TiAl合金铸件的热处理组织调控机制

Mechanisms of Microstructure Control Using Heat Treatments of TiAl Alloy Castings

余稳 徐永东 朱秀荣 王俊升 刘辰 付玉 王荫洋 李雷 韩俊刚 王宇
航空制造技术2024,Vol.67Issue(14) :51-58.DOI:10.16080/j.issn1671-833x.2024.14.051

TiAl合金铸件的热处理组织调控机制

Mechanisms of Microstructure Control Using Heat Treatments of TiAl Alloy Castings

余稳 1徐永东 1朱秀荣 1王俊升 2刘辰 1付玉 1王荫洋 1李雷 1韩俊刚 1王宇1
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作者信息

  • 1. 中国兵器科学研究院宁波分院,宁波 315103
  • 2. 北京理工大学,北京 100081
  • 折叠

摘要

TiAl合金铸态组织粗大,致使其铸件强度低、塑性差,必须通过热处理细化铸态组织.利用OM和SEM研究了Ti-47Al-2Cr-2Nb合金铸件不同热处理组织演变规律,优化制定了双态和近片层组织热处理工艺,实现了晶粒细化,揭示了细化机理.结果表明,1185℃/6 h/炉冷双态组织热处理和 1185℃/6 h/炉冷+1330℃/0.25 h/炉冷近片层组织热处理可分别将铸态组织晶粒尺寸细化 75.51%和 40.21%.双态组织热处理晶粒细化机制是在片层团晶粒内部析出大量γ晶粒打断原始粗大的片层团晶粒,γ晶核在片层团晶粒内形核来源于Al元素偏析和γ片层连续粗化.近片层组织热处理晶粒细化机制是在α单相区短时保温时发生了γ→α转变,破坏了原始粗大的片层团晶粒.等轴γ晶粒对α晶粒长大有钉扎作用,使得冷却后形成的片层团晶粒尺寸较小.

Abstract

The as-cast microstructures of TiAl alloys have low strength and poor plasticity due to their coarse grains,and they must be refined by heat treatment.The microstructure evolutions of Ti-47Al-2Cr-2Nb alloy castings after different heat treatments were studied using OM and SEM.The heat treatments of duplex(DP)and nearly lamellar(NL)microstructures were optimized and established,which realized the grain refinement.The mechanisms of grain refinement were revealed.The results show that the DP microstructure heat treatment of 1185℃/6 h/furnace cooling and the NL microstructure heat treatment of 1185℃/6 h/furnace cooling+1330℃/0.25 h/furnace cooling can refine the as-cast grain size by 75.51%and 40.21%,respectively.The grain refinement mechanism of DP microstructure heat treatment is that a large number of γ grains precipitate inside the lamellar colony grains and break the original coarse lamellar colony grains.The nucleation of γ nuclei in the lamellar colony grains comes from Al element segregation and continuous coarsening of γ lamellae.The grain refinement mechanism of NL microstructure heat treatment is that the γ→α transformation takes place in the α single phase region for a short time which destroys the original coarse lamellar colony grains,and the equiaxed γ grains can pin the growth of α grains,so that the lamellar colony grains formed after cooling are smaller.

关键词

TiAl合金铸件/热处理/双态组织/近片层组织/晶粒细化

Key words

TiAl alloy castings/Heat treatment/Duplex microstructure/Nearly lamellar microstructure/Grain refinement

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出版年

2024
航空制造技术
北京航空制造工程研究所

航空制造技术

CSTPCD北大核心
影响因子:0.403
ISSN:1671-833X
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