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粉末冶金TC11钛合金的热等静压制备与高周疲劳性能研究

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粉末热等静压(HIP)技术可以近净成形高性能钛合金复杂构件,在航空航天领域具有广阔的应用前景.采用无坩埚感应熔炼超声气体雾化法制备了TC11 预合金粉末,并对预合金粉末进行表征;在 940℃/140 MPa/3 h条件下HIP成形了TC11 坯体.采用OM、SEM、拉伸、冲击和旋转弯曲疲劳等手段对HIP坯体的显微组织和力学性能进行表征,研究了微气孔对HIP坯体疲劳性能的影响.结果表明,HIP坯体接近理论全致密,组织细小均匀,静力学性能接近甚至部分指标超越锻造合金,旋转弯曲高周疲劳强度(107 周次)为 590 MPa;空心粉形成的微气孔导致高周疲劳寿命呈现二重性,疲劳加载条件下,表面微气孔会优先成为裂纹萌生的位置,显著降低HIP坯体的高周疲劳寿命.
Powder Metallurgy TC11 Titanium Alloy Via Hot Isostatic Pressing:Preparation,Microstructure and High-Cycle Fatigue Property
Powder metallurgy through hot isostatic pressing(HIP)route,which is a promising near-net forming method,can fabricate high-performance titanium alloy components with complex structure for applications in the aerospace field.In this study,TC11 pre-alloyed powder was made by electrode induction melting gas atomization method,and the as-received powder was characterized.The powder compacts were HIP at 940℃/140 MPa/3 h from the pre-alloyed powder.The microstructure of as-HIPed powder compact was observed by OM and SEM,and the mechanical properties were evaluated by tensile,impact and high-cycle fatigue tests.The effect of residual micro-pores induced by the hollow powder with gas bubbles on fatigue life of as-HIPed powder compact was also investigated.The results show that the TC11 powder compact is approaching to full density,and the microstructure is fine and homogeneous.The quasi-static mechanical properties of as-HIPed powder compacts are close to or even better than those of wrought alloys.The rotating bending fatigue strength is about 590 MPa at 107 cycles.However,the duality of the high-cycle fatigue S-N curve is observed.The micro-pores located at the surfaces of specimens will preferentially become crack initiation sites under fatigue loading conditions,which will further significantly reduce the high-cycle fatigue life of the powder compacts.

Powder metallurgyHot isostatic pressing(HIP)TC11 titanium alloyMicrostructureFatigue property

郭瑞鹏、程敏、卢正冠、徐磊

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太原理工大学,太原 030024

中国科学院金属研究所师昌绪先进材料创新中心,沈阳 110016

粉末冶金 热等静压 TC11钛合金 显微组织 疲劳性能

国家自然科学基金国家自然科学基金山西省应用计划研究项目山西省应用计划研究项目

5220540752401104202203021221072202203021212237

2024

航空制造技术
北京航空制造工程研究所

航空制造技术

CSTPCD北大核心
影响因子:0.403
ISSN:1671-833X
年,卷(期):2024.67(17)