首页|离子色谱法测定锡膏卤素(F-、Cl-、Br-、I-)含量的不确定度评定

离子色谱法测定锡膏卤素(F-、Cl-、Br-、I-)含量的不确定度评定

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对离子色谱法测定锡膏卤素(F-、Cl-、Br-、I-)含量的不确定度进行评定.按照《化学分析测量不确定度评定》(JJF 1135-2005)和《测量不确定度评定与表示》(JJF 1059.1-2012)中的有关规定,建立锡膏卤素(F-、Cl-、Br-、I-)不确定度建立数学模型.测量不确定度的主要来源包括:标准物质纯度、标准曲线拟合、样品处理、天平称量、测量重复性和数据修约引入的不确定度,并对各个不确定度分量进行计算合成.锡膏中卤素(F-、Cl-、Br-、I-)含量测量不确定度的准确评定,有助于控制锡膏卤素的检测质量.
Uncertainty Evaluation of Determination of Content Halogen(F-,Cl-,Br-,I-)in Solder Paste by ion Chromatography
The uncertainty of the determination of halogen(F-,Cl-,Br-,I-)content in solder paste by ion chromatography was evaluated.According to the assay for the determination of the JJF 1135-2005 Evaluation of Uncertainty in Chemical Analysis Measurement and JJF 1059.1-2012 Evaluation and Expression of Uncertainty in Measurement,a mathematical model to evaluate and analyze the source of uncertainty for the determination of halogens in solder paste was established.The sources of uncertainty included the preparation of standard solutions,the fitting of calibration curve,the preparation of sample,the balance weighing,the repeatability measurement,and rounding off data,and each component of uncertainty was calculated and synthesized.The accurate assessment of the uncertainty of the content of halogens in solder paste is helpful to control the testing quality of products.

solder pasteion chromatographyhalogen contentuncertainty

李丽、韩红兰、段泽平、魏梦霞、黄慧兰、秦俊虎、熊晓娇

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云南锡业新材料有限公司,云南昆明 650500

锡膏 离子色谱色谱法 卤素含量 不确定度

2024

湖南有色金属
湖南有色金属研究院,湖南有色金属学会

湖南有色金属

影响因子:0.393
ISSN:1003-5540
年,卷(期):2024.40(2)
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