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干、湿法消解-火焰原子吸收法测定多种食品中钙元素的含量

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经干法灰化、湿式消解两种方法预处理,运用火焰原子吸收法测定多种食品中钙元素的含量。结果表明,钙元素在(1~10)μg·mL-1范围内,线性关系良好,相关系数为0.9932。所测13种食品中,虾皮的钙含量最高,为766.61mg/100g(湿法),香菇的钙含量最低,为5.16mg/100g(湿法)。干法灰化加标回收率在90.20%~103.20%,湿法消解加标回收率在90.50%~104.95%,两者相对标准偏差均小于4%。
Determination of the calcium content in foods by dry ssh and wet digestion-flame atomic absorption spectrophotometry
To determine of Calcium content in the foods,both dry ash and wet digestion methods were used. There was good linear relationship in the range of 1~10μg·mL-1 with a regression coefficient of 0.9932.The results showed that among all the samples dried small shrimps had the highest content of Calcium which was 766.61mg/100g, while the content of Calcium in Lentinula edodes was the lowest which was 5.16mg/100g. The recovery rate of dry ash samples was 90.20% to 103.20%, while wet digestion samples was 90.50% to 104.95%. RSD values of two methods were all lower than 4%.

flame atomic absorption spectrophotometrydry ashwet digestioncontent of calcium

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唐山学院 环境与化学工程系,河北 唐山 063000

火焰原子吸收 干法灰化 湿法消解 钙含量

2015

化学工程师
黑龙江省化工研究院

化学工程师

CSTPCD
影响因子:0.243
ISSN:1002-1124
年,卷(期):2015.(11)
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