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电感耦合等离子体发射光谱法测定土壤中7种金属元素

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建立了微波消解-电感耦合等离子体发射光谱法同时测定土壤中Cu、Pb、Ni、Co、Sn、Cr和Mo的分析方法.7 种金属元素在 0.05~60.0mg·L-1 浓度范围内线性关系良好,相关系数均在 0.999 以上,方法检出限范围为 0.005~0.026mg·kg-1,加标回收率在91.0%~103.0%之间;精密度RSD(n=6)均小于 5.0%.本方法前处理操作简便快捷,样品测试准确度和精密度好,可用于大批量土壤中多种元素的同时分析.
Determination of 7 metal elements in soil by ICP-AES
A method for simultaneous determination of Cu,Pb,Ni,Co,Sn,Cr and Mo in soil by microwave digestion and inductively coupled plasma emission spectrometry was established.The linear relationships of the seven metal elements were good in the range of 0.05~60.0mg·L-1,and the correlation coefficients were all above 0.999.The detection limit of the method was 0.005~0.026mg·kg-1,and the recoveries were in the range of 91.0%~103.0%.Precision RSD(n=6)were all less than 5.0%.The method has the advantages of simple and fast pretreatment operation,good sample test accuracy and precision,and can be used for simultaneous analysis of multiple elements in large quantities of soil.

soilmicrowave digestioninductively coupled plasma emission spectrometryheavy metalsresidue

李旭霞

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山东科泰环境监测有限公司,山东 临沂 276007

土壤 微波消解 电感耦合等离子体发射光谱法 重金属 残留

2024

化学工程师
黑龙江省化工研究院

化学工程师

CSTPCD
影响因子:0.243
ISSN:1002-1124
年,卷(期):2024.38(6)
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