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ICP-MS法同时测定地表水中10种痕量金属元素

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本文建立电感耦合等离子体质谱(ICP-MS)同时测定地表水中 10 种痕量金属元素残留的方法.10 种金属元素在 1.00~80.0μg·L-1 浓度范围内具有较好的线性关系,相关系数均大于 0.999,方法测定标准样品的结果均在保证值范围内,相对标准偏差均小于 4%(n=6),样品加标回收率为 87.8%~105.5%.本方法可同时进行多种金属元素的快速分析,检出限低,灵敏度高,测试结果准确,可用于地表水中铜、铅、镉、钼、铬等金属残留的分析.
Simultaneous determination of 10 trace metal elements in surface water by ICP-MS
A method for simultaneous determination of 10 trace metal residues in surface water by inductively coupled plasma mass spectrometry(ICP-MS)has been developed.The 10 metal elements had good linear relationship in the range of 1.00~80.0μg·L-1,and the correlation coefficients were all greater than 0.999.The results of the method were all within the guaranteed value range,the relative standard deviations were all less than 4%(n=6),and the recoveries of the samples were 87.8%~105.5%.With low detection limit,high sensitivity and accurate test results,this method can be used for the analysis of copper,lead,cadmium,molybdenum,chromium and other metal residues in surface water.

inductively coupled plasma mass spectrometrysurface watermetallic elementresidual

赵飞燕

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河南省安阳水文水资源勘测局,河南 安阳 455000

电感耦合等离子体质谱 地表水 金属元素 残留

2024

化学工程师
黑龙江省化工研究院

化学工程师

CSTPCD
影响因子:0.243
ISSN:1002-1124
年,卷(期):2024.38(7)