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气相色谱-质谱法测定沥青基耐穿刺防水卷材中的阻根剂

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建立了气相色谱-质谱法测定沥青基耐穿刺防水卷材中3种阻根剂的方法,内标法定量。样品通过二氯甲烷超声提取,前处理时间短,操作简单。在10~150mg·L-1浓度范围内线性关系良好,相关系数均大于0。99,0。3%加标水平的回收率为98。6%~114。2%,精密度为1。08%~1。65%。该方法快速、准确,可以满足沥青基耐穿刺防水卷材中阻根剂含量测定的需要。
Determination of root inhibitor in asphalt based waterproof coiled material by GC-MS
A GC-MS method for the determination of three kinds of root inhibitors in asphalt-based waterproof coiled material was established,and the internal standard method was used for quantifincation.The samples were extracted by ultrasonic extraction of methylene chloride.The pretreatment time was short and the operation was simple.In the concentration range of 10~150mg·L-1,the linearity ship was good,and the correlation coefficients were all greater than 0.99.The recoveries at the 0.3%spiked level were 98.6%~114.2%and the precision was 1.08%~1.65%.The method is fast and accurate,and can meet the need of the content determination of root inhibitor asphalt based waterproof coiled material.

GC-MSasphalt-based waterproof coiled materialroot inhibitorinternal standard method

祁魁、李建兵、张毅、张艳艳、吴龙

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青岛市产品质量检验研究院,山东 青岛 266101

国家海洋精细化工及生物制品质量检验检测中心,山东青岛 266101

气相色谱-质谱法 沥青基耐穿刺防水卷材 阻根剂 内标法

2024

化学工程师
黑龙江省化工研究院

化学工程师

CSTPCD
影响因子:0.243
ISSN:1002-1124
年,卷(期):2024.38(12)