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单晶SiC基片干式摩擦化学机械抛光初探

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针对碳化硅(SiC)基片在抛光过程中效率低、费用高、环境污染大等问题,提出了一种在干式状态下对SiC基片进行摩擦化学机械抛光的方法(dry tribochemical mechanical polishing,DTCMP).探究不同工艺参数(磨料种类、磨粒粒径、磨粒含量、抛光盘转速、抛光载荷、固相氧化剂含量)对单晶SiC基片抛光效率和表面质量的影响规律.研究结果表明:金刚石磨粒更适合SiC的摩擦化学机械抛光;当磨粒粒径为W1,磨粒质量为 4 g,抛光盘转速为 70 r/min,抛光载荷为 20.685 kPa,固相氧化剂过碳酸钠添加量为 10 g时,其为最优工艺参数.采用最优工艺参数对表面粗糙度约为 20 nm的单晶 6H-SiC基片进行干式抛光加工,最终获得表面粗糙度Ra为 3.214 nm.DTCMP方法抛光SiC基片比水基抛光法热量损失少,所产生的界面温度更高,反应所需的活化能更低,可以实现SiC基片的绿色、高效和高质量抛光.
Preliminary investigation of dry tribochemical mechanical polishing of single crystal SiC substrates
Aiming at the issues of low efficiency,high cost,and environmental pollution associated with silicon carbide(SiC)substrates in the polishing process,a method of tribochemical mechanical polishing of SiC substrates in the dry state(Dry Tribochemical Mechanical Polishing,DTCMP)is proposed.The effect of different process parameters(abras-ive type,abrasive size,abrasive content,polishing plate speed,polishing load,solid phase oxidant content)on the pol-ishing efficiency and surface quality of single-crystal silicon carbide substrates was investigated.The results show that diamond abrasive is more suitable for the tribochemical mechanical polishing of silicon carbide.Optimal test paramet-ers are achieved when the abrasive size is W1,the abrasive content is 4 g,the polishing plate speed is 70 r/min,the pol-ishing load is 20.685 kPa,and the solid phase oxidant sodium percarbonate is added at 10 g.Single-crystal 6H-SiC sub-strates with a surface roughness of approximately 20 nm were polished using the optimal process parameters,finanlly resulting in a surface roughness of Ra of 3.214 nm.The DTCMP method for polishing SiC substrate has less heat loss than water-based polishing method,enabling higher interface temperature and lower activation energy required for reac-tions.This method can realize green,efficient and high-quality polishing of SiC substrates.

SiC substratedry tribochemical mechanical polishingmaterial removal ratesurface roughness

薛明普、肖文、李宗唐、王占奎、苏建修

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河南科技学院 机电学院, 河南 新乡 453003

SiC基片 干式摩擦化学机械抛光 材料去除率 表面粗糙度

2024

金刚石与磨料磨具工程
郑州磨料磨具磨削研究所

金刚石与磨料磨具工程

CSTPCD北大核心
影响因子:0.354
ISSN:1006-852X
年,卷(期):2024.44(1)
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