首页|结合剂比例和cBN粒度配比对PcBN复合材料微观结构和性能的影响

结合剂比例和cBN粒度配比对PcBN复合材料微观结构和性能的影响

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在高温高压条件下制备了聚晶立方氮化硼(PcBN)复合材料.采用X射线衍射(XRD)、扫描电子显微镜(SEM)、能谱仪(EDS)等研究了结合剂配比和立方氮化硼(cBN)粒度对PcBN复合材料的成分、微观结构、显微硬度和磨耗比的影响.实验结果表明:在压力5.5 GPa,温度1400 ℃,保温10min的烧结条件下,当V(TiN0.3)∶V(AlN)=70∶30时,PcBN复合材料性能较为优异,硬度最高达到22.7 GPa,磨耗比达到149.2;当PcBN复合材料中cBN粒度组合为V(0.5~1 μm)∶V(2~5 μm)∶V(5~10 μm)=3∶5∶2时,颗粒之间的堆积密度达到最高,性能也达到最优.
Effects of the ratio of binder and the ratio of cBN particle size on the microstruc-ture and properties of PcBN composites
Polycrystalline cubic boron nitride composites were prepared under high-temperature and high-pressure con-ditions.The effects of bonding agent ratio and cBN particle size on the composition,microstructure,microhardness,and abrasive ratios of the PcBN composites were investigated using X-ray diffraction(XRD),field scanning electron micro-scopy(SEM),and energy dispersive spectroscopy(EDS).The experimental results showed that the PcBN composites performed better under sintering conditions of 5.5 GPa,1 400 ℃,and a 10-minute holding time,achieving a hardness of up to 22.7 GPa and an abrasion ratio of 149.2 at V(TiN0.3)∶V(AlN)=70∶30.Moreover,when the particle size combina-tion of cBN in PcBN composites is(0.5~1)μm∶(2~5)μm∶(5~10)μm=3∶5∶2,the packing density between particles reaches its peak,resulting in optimal performance.

PcBN compositehigh pressure and high temperature(HPHT)binderparticle size

邹芹、董培航、李艳国、袁振雄、武迪、罗永安

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燕山大学,亚稳材料制备技术与科学国家重点实验室,河北秦皇岛 066004

燕山大学机械工程学院,河北秦皇岛 066004

PcBN复合材料 高温高压 结合剂 粒度

河北省高等学校科学技术研究项目

ZD2021099

2024

金刚石与磨料磨具工程
郑州磨料磨具磨削研究所

金刚石与磨料磨具工程

CSTPCD北大核心
影响因子:0.354
ISSN:1006-852X
年,卷(期):2024.44(2)
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