首页|一步合成纳米CuO及其催化降解玫瑰红B染料废水的应用研究

一步合成纳米CuO及其催化降解玫瑰红B染料废水的应用研究

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采用以硝酸铜、氨水和氢氧化钠为原料的沉淀法,一步合成出纳米CuO,并进一步考察这些材料对催化过氧化氢分解玫瑰红B染料废水的脱色性能.通过XRD、N2-吸附脱附及SEM等表征手段对纳米CuO的结构进行表征.XRD 结果表明,所获样品均为具有单斜晶体结构的纳米CuO.N2-吸附脱附结果表明,纳米CuO是介孔结构,孔径多集中分布在 3~4nm处.SEM结果表明,合成的纳米CuO为球状,且由大量的纳米CuO薄片自组装而成.脱色率测试结果表明,纳米CuO对催化H2O2 降解玫瑰红B染料废水具有较好的效果,反应约 2h的脱色率可达 97%.
Study on One-Step Synthesis of Nano-CuO and its Catalytic Degradation of Rose Red B Dye Wastewater
Nano-cuo was synthesized in one step by the precipitation method with copper nitrate,ammonia and sodium hydroxide as raw materials.The decolorization performance of these materials on rose B dye wastewater catalyzed by hydrogen peroxide was further investigated.The structure of nano-CuO was characterized by XRD,N2-adsorption desorption and SEM.XRD results show that all the samples are nano-CuO with monoclinic crystal structure.The results of N2-adsorption and desorption show that the nano-CuO is mesoporous structure,and the pore size is mainly distributed at 3~4nm.The SEM results show that the nano-CuO is spherical and self-assembled by a large number of nano-CuO sheets.The results of decolorization test show that nano-CuO has a good effect on the degradation of rose red B dye wastewater by H2O2,and the decolorization rate can reach 97%after the reaction of about 2h.

one-step methodnano-copper oxidecatalyzerose B dye wastewater

谢锦文、李文、李攀荣、王佳琪

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江西金达莱环保股份有限公司,江西南昌,330199

一步合成 纳米CuO 催化 玫瑰红B染料废水

江西省重大科技计划项目

2019BCD41002

2024

江西化工
江西化学化工学会 江西省化学工业研究所

江西化工

影响因子:0.272
ISSN:1008-3103
年,卷(期):2024.40(1)
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