计量与测试技术2024,Vol.51Issue(1) :6-9.DOI:10.15988/j.cnki.1004-6941.2024.1.002

果蔬汁中有机磷农药残留能力验证结果与分析

Validation Results and Analysis of Organophosphorus Pesticide Residues in Fruit and Vegetable Juice

刘贺 张鹏 刘宁 刘一鸣 马玲 彭菲
计量与测试技术2024,Vol.51Issue(1) :6-9.DOI:10.15988/j.cnki.1004-6941.2024.1.002

果蔬汁中有机磷农药残留能力验证结果与分析

Validation Results and Analysis of Organophosphorus Pesticide Residues in Fruit and Vegetable Juice

刘贺 1张鹏 1刘宁 1刘一鸣 1马玲 1彭菲1
扫码查看

作者信息

  • 1. 满洲里海关技术中心
  • 折叠

摘要

为了监测实验室有机磷农药残留检测能力,参加全国范围内能力验证.该实验根据GB 23200.116-2019国家标准,并对其方法进行简单优化.对于单一阳性样品,取两次平行检测的平均值,添加已知浓度的标准品,并计算回收率,减少基质效应对结果的影响.结果表明:有机磷农药残留能力验证结果满意,且实验室满足检测要求,确保了检测结果的可靠性;优化后,实验操作简单,可用于实验室日常快速检测有机磷类农药.

Abstract

To monitor laboratory organophosphorus pesticide residue detection capability,participate in nationwide capability verification.The experiment is based on GB 23200.116-2019 national standard,and its method is sim-ply optimized.For a single positive sample,the average of two parallel tests was taken,the standard substance of known concentration was added,and the recovery rate was calculated to reduce the influence of matrix effect on the results.The results showed that the verification results of organophosphorus pesticide residue capability were satis-factory,and the laboratory met the detection requirements,which ensured the reliability of the detection re-sults.After optimization,the experimental operation is simple,and it can be used for daily rapid detection of organ-ophosphorus pesticides in the laboratory.

关键词

能力验证/有机磷/马拉硫磷/甲胺磷/气相色谱法

Key words

capability verification/organic phosphorus/malathion/methamidophos/gas chromatography

引用本文复制引用

基金项目

海关总署科研项目(2022HK029)

出版年

2024
计量与测试技术
成都市计量监督检定测试所

计量与测试技术

影响因子:0.175
ISSN:1004-6941
参考文献量16
段落导航相关论文