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滤膜中铅质控样品的研制

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针对滤膜中铅质控样品,提出一种制备和定值方法.将混合纤维素空白滤膜作为基质,采用标准体积添加方式进行制备,再用火焰原子吸收分光光度法进行均匀性和稳定性评估,并进行不确定度评定.结果表明:该方法具有可行性,且样品的均匀性和稳定性较好,量值和不确定度符合使用要求,可为其检测方法及数据有效性的评价提供参考.
Preparation of Quality Control Sample for Lead Determination in Filter Membrane Material
A method of preparation and determination of lead quality control samples in filter membrane was pro-posed.The mixed cellulose blank filter membrane was prepared by the standard volume addition method,and then the uniformity and stability were evaluated by flame atomic absorption spectrophotometry,and the uncertainty was e-valuated.The results show that the method is feasible,and the sample uniformity and stability are good,the magni-tude and uncertainty meet the requirements of use,and can provide a reference for the evaluation of the detection method and the validity of the data.

leadheavy metalfilter membranequality control sampleuncertainty

李娅、陈杨、黎晓玲

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湖南省计量检测研究院

重金属 滤膜 质控样品 不确定度

2024

计量与测试技术
成都市计量监督检定测试所

计量与测试技术

影响因子:0.175
ISSN:1004-6941
年,卷(期):2024.50(11)