高品质月桂酰氯的合成研究
Study on the Synthesis of High-quality Dodecanoyl Chloride
陈郭芹 1刘国文 1王喆 1兰世林 1周嘉良 1臧阳陵 1杜升华1
作者信息
- 1. 湖南化工研究院有限公司 国家农药创制工程技术研究中心,湖南长沙 410014;农用化学品湖南省重点实验室,湖南长沙 410014
- 折叠
摘要
以3-甲基吡啶为催化剂,月桂酸与光气反应合成高品质月桂酰氯,优化条件下,产品纯度≥99.5％,收率＞98.0％(以月桂酸计),色度＜5.该方法操作简单,无溶剂,产品收率和纯度高,色度低,无异味,品质稳定,杂质少,生产成本低,适合于工业化生产.
Abstract
Using 3-methylpyridine as a catalyst,lauric acid and phosgene were reacted to synthesize high quality dodecanoyl chloride with yield＞98.0％(measured by lauric acid),purity ≥99.5％,and chroma＜5.The method has the advantages such as simple operation,no solvent requirement,high yield and purity,low chroma,absence of extraneous odour,stable quality,fewer impurities and low production cost,making it suitable for industrial production.
关键词
月桂酸/光气/月桂酰氯/3-甲基吡啶Key words
lauric acid/phosgene/dodecanoyl chloride/3-methylpyridine引用本文复制引用
出版年
2024
NETL
NSTL
万方数据